4-甲氧基-3-羟基苯乙酮合成路线 (共 31 条)
反应条件
1: With AlCl3, aluminium chloride in dichloromethane T=18°C; 24 h; 2: With water in dichloromethane
参考文献
CRYPTOPHARMA PTY LTD
Patent: WO2008/124878 A1, 2008 ;
Location in patent: Page/Page column 38 ;
反应条件
lithium carbonate in N,N-dimethyl-formamide T=55°C; 18 h;
参考文献
Wymann, Walter E.; Davis, Roman; Patterson, John W.; Pfister, Juerg R.
Synthetic Communications, 1988 , vol. 18, # 12 p. 1379 - 1384
反应条件
hydrogen bromide 3 h; Heating;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 21, # 3 p. 186 - 188
反应条件
sulfuric acid T=65°C; 20 h;
参考文献
Rosiak, Anna; Frey, Wolfgang; Christoffers, Jens
European Journal of Organic Chemistry, 2006 , # 17 p. 4044 - 4054
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
Heterocycles, , vol. 44, # 1 p. 139 - 142
反应条件
carbon disulfide; aluminium trichloride
参考文献
Helvetica Chimica Acta, , vol. 10, p. 389
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,4-dioxane 1 h;
参考文献
Synthesis, , # 20 p. 3389 - 3396
反应条件
1: 85 percent / tetrahydrofuran / 5 - 20 °C 2: DDQ / dioxane / 1 h View Scheme
参考文献
Synthesis, , # 20 p. 3389 - 3396
反应条件
chloroacetic acid T=180 - 190°C;
参考文献
DE674517 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 24, p. 225
反应条件
aluminum tri-bromide in 1,2-dichloro-benzene 22 h; Ambient temperaturevarious amounts of AlBr3; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 102, # 9 p. 3056 - 3062