2-乙酰基-4-戊酸乙酯合成路线 （共 58 条）
反应条件
potassium carbonate in tetrahydrofuran T=70°C; Tsuji-Trost Allylation; 18 h; Schlenk technique; Reagent/catalystTemperatureTime;
参考文献
Dickschat, Arne T.; Behrends, Frederik; Surmiak, Sabrina; Weiss, Mark; Eckert, Hellmut; Studer, Armido
Chemical Communications, 2013 , vol. 49, # 22 p. 2195 - 2197
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=100°C; 4 h;
参考文献
Bergbreiter, David E.; Weatherford, David A.
Journal of the Chemical Society, Chemical Communications, 1989 , # 13 p. 883 - 884
反应条件
lithium hydroxide hydrate in water T=20°C; 0.25 h; Sonication;
参考文献
Pancote, Camila G.; De Carvalho, Bruno S.; Luchez, Cibele V.; Fernandes, Joao P.S.; Politi, Mario J.; Brandt, Carlos A.
Synthesis, 2009 , # 23 art. no. M02309SS, p. 3963 - 3966
反应条件
P(MeNCH2CH2)3N in hexane; acetonitrile T=0°C; 0.5 h;
参考文献
Arumugam, Subramaniam; McLeod, Dale; Verkade, John G.
Journal of Organic Chemistry, 1998 , vol. 63, # 11 p. 3677 - 3679
反应条件
pyridine; magnesium sulfate; 1,2-(p-MeOC6H4)2cyclobuten[=P(2,4,6-tri-t-BuPh)]2PdOTf T=50°C; 3 h;
参考文献
Journal of the American Chemical Society, , vol. 124, # 37 p. 10968 - 10969
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate in tetrahydrofuran T=70°C; Tsuji-Trost Allylation; 18 h; Schlenk technique;
参考文献
Dickschat, Arne T.; Behrends, Frederik; Surmiak, Sabrina; Weiss, Mark; Eckert, Hellmut; Studer, Armido
Chemical Communications, 2013 , vol. 49, # 22 p. 2195 - 2197
反应条件
potassium carbonate in tetrahydrofuran T=70°C; Tsuji-Trost Allylation; 20 h;
参考文献
Noda, Hiroto; Motokura, Ken; Miyaji, Akimitsu; Baba, Toshihide
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 5 p. 973 - 980
反应条件
1: ethyl acetoacetate With sodium hydride in tetrahydrofuran T=25°C; 0.5 h; 2: ethylene,methyl acetate With bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in tetrahydrofuran T=25°C; 20 h; Title compound not separated from byproducts;
参考文献
Synthesis, , # 15 p. 2320 - 2326
反应条件
ammonium cerium(IV) nitrate in methanol 0.333333 h; Ambient temperature;
参考文献
Hwu, Jih Ru; Chen, Chung Nan; Shiao, Shui-Sheng
Journal of Organic Chemistry, 1995 , vol. 60, # 4 p. 856 - 862
反应条件
1: in acetonitrile T=20°C; 2: With triethylamine in hexane; ethyl acetate T=20°C; 0.5 h;
参考文献
Journal of Organic Chemistry, , vol. 69, # 19 p. 6267 - 6272
