iron(III) chloride; nitrogen(IV) oxide; ozone in 1,2-dichloro-ethane T=5°C; Kyodai nitration; 1.5 h;

hydrogenchloride

hydrogenchloride T=20°C;

暂无反应条件数据

hydrogenchloride; zinc anschl. mit aethanol. Natriumaethylat;

1: zinc-dust; ethanolic HCl / anschl. mit aethanol. Natriumaethylat 2: hydrochloric acid View Scheme

1: zinc-dust; ethanolic HCl / anschl. mit aethanol. Natriumaethylat 2: 180 - 200 °C View Scheme

1.1: hydrogen / palladium 10 on activated carbon / methanol / 40 °C / 3102.97 Torr / Industry scale 2.1: potassium carbonate / potassium iodide / isobutyramide / 60 - 90 °C / Industry scale 3.1: lithium aluminium tetrahydride / tetrahydrofuran / 20.5 h / -50 - 20 °C / Industry scale 3.2: 15 °C / Industry scale 4.1: thionyl chloride / acetonitrile / 5 - 18 °C / Industry scale 5.1: potassium hydroxide / toluene; water / 0.33 h / 12.5 °C / Industry scale; Inert atmosphere 5.2: 1.65 h / 12.5 - 14.6 °C / Industry scale; Inert atmosphere 6.1: (9R)-1-[3,5-bis(trifluoromethyl)benzyl]cinchonan-1-ium-9-ol bromide / toluene; water / 16 h / 10 °C / Industry scale; Inert atmosphere 7.1: toluene / 6.67 h / 90 °C / Industry scale 8.1: hydrogen / palladium 10 on activated carbon / toluene; methanol / 20 - 27 °C / 3102.97 Torr / Industry scale 8.2: 20 °C / pH 6.3 / Industry scale View Scheme

1.1: palladium on activated charcoal; hydrogen / methanol / 24 h / 20 °C / |Inert atmosphere 2.1: hydrogenchloride / water / 1 h / 20 °C 2.2: 0.5 h / -10 - 5 °C 2.3: 0.5 h View Scheme

formaldehyd; propionic acid; nickel monoaluminide in methanol; water