反应条件
1: 2,4,6-trimethyl-phenol With sodium hydride in diethyl ether
Metallation; 0.5 h;
2: propiolic acid chloride in diethyl ether
T=-78°C; Acylation; 0.5 h;
参考文献
Nagel, Matthias; Hansen, Hans-Juergen
Helvetica Chimica Acta, 2000 , vol. 83, # 5 p. 1022 - 1048