4-甲氧基苯乙酰硫氰酸酯合成路线 (共 24 条)
反应条件
1: ammonium thiocyanate With montmorillonite K10 clay in acetone T=20°C; 0.666667 h; 2: 2-bromo-4'-methoxy-acetophenone T=20°C; 0.00833333 h; Neat (no solvent)Grinding;
参考文献
Meshram; Thakur, Pramod B.; Madhu Babu; Bangade, Vikas M.
Tetrahedron Letters, 2012 , vol. 53, # 14 p. 1780 - 1785
反应条件
diiodine pentaoxide in methanol T=20°C; 0.333333 h;
参考文献
Wu, Liqiang; Yang, Xiaojuan; Yan, Fulin
Journal of Sulfur Chemistry, 2011 , vol. 32, # 2 p. 105 - 110
反应条件
cerium(III) chloride in acetonitrile T=80°C; 5 h;
参考文献
Yadav; Subba Reddy; Srinivas
Chemistry Letters, 2004 , vol. 33, # 7 p. 882 - 883
反应条件
tetrabutylammomium bromide in water T=20°C; 0.416667 h;
参考文献
Sayyahi, Soheil; Saghanezhad, Jafar
Chinese Chemical Letters, 2011 , vol. 22, # 3 p. 300 - 302
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in acetonitrile T=20°C; 0.666667 h; regioselective reaction;
参考文献
Wu, Dezhen; Yang, Xiaojuan; Wu, Liqiang
Journal of Chemical Sciences (Bangalore), 2012 , vol. 124, # 4 p. 901 - 905,5
反应条件
1: 1-(4-methoxyphenyl)ethanone With PhI(ODNs)OH in acetonitrile T=80°C; 1 h; 2: [C4mim][SCN] in acetonitrile T=20°C; 0.166667 h;
参考文献
Huang, Hsin-Yu; Wang, Huey-Min; Hou, Rei-Sheu; Cheng, Hui-Ting; Chen, Ling-Ching
Journal of the Chinese Chemical Society, 2008 , vol. 55, # 6 p. 1204 - 1207
反应条件
cis-1,4-bis(triphenylphosphonium)-2-butene peroxodisulfate; oxygen in methanol T=0°C; 1 h;
参考文献
Badri, Rashid; Gorjizadeh, Maryam
Synthetic Communications, 2012 , vol. 42, # 14 p. 2058 - 2066
反应条件
in ethanol 2 h; Heating;
参考文献
Delbecq, Frederic; Cordonnier, Guy; Pommery, Nicole; Barbry, Didier; Henichart, Jean-Pierre
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 5 p. 1119 - 1121
反应条件
ammonium cerium(IV) nitrate; oxygen in methanol T=0°C; Addition; 0.5 h;
参考文献
Nair, Vijay; Nair, Latha G; George, Tesmol G; Augustine, Anu
Tetrahedron, 2000 , vol. 56, # 38 p. 7607 - 7611
反应条件
cis-1,4-bis(triphenylphosphonium)-2-butene peroxodisulfate in methanol T=20°C; 1 h;
参考文献
Synthetic Communications, , vol. 42, # 14 p. 2058 - 2066