N-(4-戊炔基)酞酰亚胺合成路线 （共 13 条）
反应条件
copper(II)-citrate; 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; hypophosphorous ether in water; N,N-dimethyl-formamide
T=130°C; 6 h; Inert atmosphereGreen chemistry; chemoselective reaction;
参考文献
Cao, Huanyang; Chen, Tieqiao; Zhou, Yongbo; Han, Daoqing; Yin, Shuang-Feng; Han, Li-Biao
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 4 p. 765 - 769
反应条件
1: 37 percent / Pd(OAc)2; CuI; DABCO / air / acetonitrile / 10 h / 20 °C
2: 70 percent / NH2NH2*H2O / ethanol; tetrahydrofuran / 3 h / 60 °C
View Scheme
参考文献
Dautel, Olivier J.; Robitzer, Mike; Lere-Porte, Jean-Pierre; Serein-Spirau, Francoise; Moreau, Joel J. E.
Journal of the American Chemical Society, 2006 , vol. 128, # 50 p. 16213 - 16223
反应条件
formic acid; F6P(1-)*C16H22N3Ru(1+); water in 1-methyl-pyrrolidin-2-one
T=25°C; 48 h; Inert atmosphereSealed tube;
参考文献
Zeng, Mingshuo; Li, Le; Herzon, Seth B.
Journal of the American Chemical Society, 2014 , vol. 136, # 19 p. 7058 - 7067
