2-(4-甲基苄基)呋喃合成路线 (共 11 条)
反应条件
triphenyl phosphite; benzyltrimethylammonium diphenylphosphinate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; copper(l) iodide in various solvent(s)
12 h; Ambient temperature;
参考文献
Zhang, Shijie; Marshall, Daniel; Liebeskind, Lanny S.
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2796 - 2804
反应条件
triphenyl phosphite; potassium carbonate; bis(benzonitrile)palladium(II) dichloride in tetrahydrofuran
48 h; Ambient temperature;
参考文献
Zhang, Shijie; Marshall, Daniel; Liebeskind, Lanny S.
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2796 - 2804
反应条件
1: 49 percent / HPF6 / diethyl ether; H2O / 1 h / 0 °C
2: 55 percent / (PhO)3P, K2CO3 / (PhCN)2PdCl2 / tetrahydrofuran / 48 h / Ambient temperature
View Scheme
参考文献
Zhang, Shijie; Marshall, Daniel; Liebeskind, Lanny S.
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2796 - 2804
反应条件
triphenyl phosphite; zinc(II) chloride; bis(benzonitrile)palladium(II) dichloride
1) ether, 5-20 deg C, 30 min, 2) ether-hexane-THF, 20 deg C, 36 h; Yield givenMultistep reaction;
参考文献
Zhang, Shijie; Marshall, Daniel; Liebeskind, Lanny S.
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2796 - 2804
反应条件
triphenyl phosphite; benzyltrimethylammonium diphenylphosphinate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; copper(l) iodide in various solvent(s)
12 h; Ambient temperatureother reagents (LiCl, NaOAc), other solvents (THF); Product distribution;
参考文献
Zhang, Shijie; Marshall, Daniel; Liebeskind, Lanny S.
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2796 - 2804
参考文献
Mndshojan et al.
Doklady Akademii Nauk Armyanskoi SSR, 1958 , vol. 27, p. 305,308
Chem.Abstr., 1960 , p. 481
反应条件
lithium sodium; ammonia; lithium
1.) ether; Yield given. Multistep reaction;
参考文献
Hall; Farahat
Journal of Heterocyclic Chemistry, 1987 , vol. 24, # 4 p. 1205 - 1213
反应条件
1: aluminium chloride
2: aq. NaOH solution
3: 230 °C / Erhitzen
View Scheme
参考文献
Mndshojan et al.
Doklady Akademii Nauk Armyanskoi SSR, 1958 , vol. 27, p. 305,308
Chem.Abstr., 1960 , p. 481
反应条件
1: aq. NaOH solution
2: 230 °C / Erhitzen
View Scheme
参考文献
Mndshojan et al.
Doklady Akademii Nauk Armyanskoi SSR, 1958 , vol. 27, p. 305,308
Chem.Abstr., 1960 , p. 481
反应条件
1: aluminium chloride
2: aq. NaOH solution
3: 230 °C / Erhitzen
View Scheme
参考文献
Mndshojan et al.
Doklady Akademii Nauk Armyanskoi SSR, 1958 , vol. 27, p. 305,308
Chem.Abstr., 1960 , p. 481