in tetrahydrofuran 12 h; sealed tube, bath temperature 250 deg C;
参考文献
Odinokov, V. N.; Akhmetova, V. R.; Tolstikov, G. A.; Moiseenkov, A. M.; Semenovskii, A. V.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 3 p. 443 - 447
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 3 p. 489 - 494
N,N,N',N',N'',N''-hexamethylphosphoric triamide; lithium hexamethyldisilazane 1.) THF, 0 deg C, 10 min, 2.) THF, 0 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kling, Marcel R.; Easton, Christopher J.; Poulos, Alf
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 10 p. 1183 - 1190
Kovalev, B. G.; Dzhumakulov, T.; Abduvakhabov, A. A.; Sadykov, A. S.
Doklady Chemistry, 1987 , vol. 297, # 12 p. 544 - 548
Dokl. Akad. Nauk SSSR Ser. Khim., 1987 , vol. 297, # 6 p. 1381 - 1386
air; sodium hexamethyldisilazane in tetrahydrofuran
1 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
N,N,N',N',N'',N''-hexamethylphosphoric triamide; lithium hexamethyldisilazane
1.) THF, 0 deg C, 10 min, 2.) THF, 0 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kling, Marcel R.; Easton, Christopher J.; Poulos, Alf
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 10 p. 1183 - 1190
Kovalev, B. G.; Dzhumakulov, T.; Abduvakhabov, A. A.; Sadykov, A. S.
Doklady Chemistry, 1987 , vol. 297, # 12 p. 544 - 548
Dokl. Akad. Nauk SSSR Ser. Khim., 1987 , vol. 297, # 6 p. 1381 - 1386