2,6-二甲基-5-庚烯-2-醇合成路线 (共 35 条)
反应条件
1: 22 percent / SOCl2, pyridine / benzene / 0 - 20 °C
2: 13 percent / tetraphenylporphine, O2 / CH2Cl2 / 2 h / -50 °C
3: triphenylphosphine
View Scheme
参考文献
Carless, Howard A.J.; Batten, Richard J.
Tetrahedron Letters, 1982 , vol. 23, # 45 p. 4735 - 4738
反应条件
Amberlyst-15 (H+) resin in toluene
T=60 - 70°C; 6 h;
参考文献
Singh, Soni A.; Kabiraj, Shilpi; Khandare, Reena P.; Nalawade, Shrikant P.; Upar, Kiran B.; Bhat, Sujata V.
Synthetic Communications, 2010 , vol. 40, # 1 p. 74 - 80
参考文献
Bateman et al.
Journal of the Chemical Society, 1952 , p. 1714,1717
参考文献
Bateman et al.
Journal of the Chemical Society, 1952 , p. 1714,1717
参考文献
Bateman et al.
Journal of the Chemical Society, 1952 , p. 1714,1717
参考文献
Bateman et al.
Journal of the Chemical Society, 1952 , p. 1714,1717
参考文献
Bateman et al.
Journal of the Chemical Society, 1952 , p. 1714,1717
参考文献
Givaudan Corporation
Patent: US4634548 A1, 1987 ;
参考文献
Harries; Weil
Chemische Berichte, 1904 , vol. 37, p. 846
反应条件
thionyl chloride; 2,3-dimethyl aniline
zuletzt bei 120grad;
参考文献
Kennedy,J.P.; Melby,E.G.
Journal of Organic Chemistry, 1975 , vol. 40, p. 1099 - 1101