2,6-二氯-1,4-苯二胺合成路线 （共 11 条）
反应条件
1: sulfuric acid 2: acetic acid; calcium hypochlorite 3: aqueous sulfuric acid 4: Diazotization.Behandlung der Diazoniumsalz-Loesung mit CuCl in wss. HCl, zuletzt bei 60grad View Scheme
参考文献
Schoutissen
Journal of the American Chemical Society, 1933 , vol. 55, p. 4541,4544
反应条件
sulfuric acid; acetic acid; potassium iodide; sodium nitrite 1.)0-5 deg C; 2.)heated; Yield given. Multistep reaction;
参考文献
Bolton, Roger; Moore, Clive; Sandall, John P.B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 1593 - 1598
反应条件
Diazotization.Behandlung der Diazoniumsalz-Loesungen mit CuCl in wss. HCl;
参考文献
Schoutissen
Journal of the American Chemical Society, 1933 , vol. 55, p. 4541,4544
参考文献
Levy
Chemische Berichte, 1883 , vol. 16, p. 1448
Chemische Berichte, 1885 , vol. 18, p. 2369
反应条件
hydrogen in tetrahydrofuran; water
T=120°C; P=37503.8 Torr; 15 h; chemoselective reaction;
参考文献
Jagadeesh, Rajenahally V.; Surkus, Annette-Enrica; Junge, Henrik; Pohl, Marga-Martina; Radnik, Joerg; Rabeah, Jabor; Huan, Heming; Schunemann, Volker; Brueckner, Angelika; Beller, Matthias
Science, 2013 , vol. 342, # 6162 p. 1073 - 1076
反应条件
hydrogenchloride; tin(ll) chloride
参考文献
Meyer, Walter E.; Tomcufcik, Andrew S.; Chan, Peter S.; Emma, John E.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 12 p. 1705 - 1710
参考文献
Witt
Chemische Berichte, 1875 , vol. 8, p. 145
反应条件
1: pyridine
2: lead (IV)-acetate
View Scheme
参考文献
Adams et al.
Journal of the American Chemical Society, 1954 , vol. 76, p. 1114,1117
参考文献
Morgan; Cleage
Journal of the Chemical Society, 1918 , vol. 113, p. 592
反应条件
pyridine
Erhitzen des Reaktionsprodukts mit wss. Salzsaeure;
参考文献
Drake et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1602,1603
