1-N-乙酰基-3-硝基对亚苯二胺合成路线 （共 23 条）
反应条件
ammonia T=10 - 15°C; durch Stehenlassen;
参考文献
Chemische Berichte, , vol. 30, p. 986
反应条件
1: acetic acid / 0.25 h / Heating 2: acetic acid / 0.25 h / Heating 3: 60percent nitric acid, conc. sulfuric acid / 1.) 0 deg C, 10 min, 2.) RT, 30 min 4: conc. sulfuric acid / 0.25 h / 100 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 38, # 10 p. 1786 - 1792
反应条件
1: acetic acid / 0.25 h / Heating 2: 60percent nitric acid, conc. sulfuric acid / 1.) 0 deg C, 10 min, 2.) RT, 30 min 3: conc. sulfuric acid / 0.25 h / 100 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 38, # 10 p. 1786 - 1792
参考文献
McFarlane, Michael D.; Moody, David J.; Smith, David M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 691 - 696
反应条件
sulfuric acid; potassium nitrate T=-10 - -5°C; und verseift das dabei entstehende N-<2-Nitro-4-acetamino-phenyl>-phthalimid durch mehrtaegiges Stehenlassen mit Ammoniak oder schneller durch wiederholtes Abdampfen mit Ammoniak;
参考文献
Chemische Berichte, , vol. 40, p. 3179,3183
反应条件
1: 60percent nitric acid, conc. sulfuric acid / 1.) 0 deg C, 10 min, 2.) RT, 30 min 2: conc. sulfuric acid / 0.25 h / 100 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 38, # 10 p. 1786 - 1792
反应条件
rat liver cytosol protein; [14C]-Acetyl-Coenzyme A T=37°C; 0.5 h; solvent: propylene glycol, Tris-HCl buffer (pH 7.5); var. arylamines, var. nitroanilines; in vitro metabolism study; Product distribution;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 38, # 9 p. 2561 - 2566
反应条件
1: concentrated sulfuric acid; KNO3 / -10 - -5 °C 2: ammonia / bei gewoehnlicher Temperatur View Scheme
参考文献
Chemische Berichte, , vol. 36, p. 413
反应条件
1: natrium carbonate / 10 °C 2: concentrated sulfuric acid; KNO3 / -10 - -5 °C 3: ammonia View Scheme
参考文献
Chemische Berichte, , vol. 36, p. 413
反应条件
1: concentrated sulfuric acid; KNO3 / -10 - -5 °C 2: ammonia View Scheme
参考文献
Chemische Berichte, , vol. 36, p. 413
