4-(二甲基氨基)苯甲酰胺合成路线 （共 21 条）
反应条件
zinc(II) chloride T=160 - 200°C;
参考文献
Bayer and Co.
Patent: DE77329 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 4, p. 173
参考文献
Baeyer and Co.
Patent: DE77329 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 4, p. 173
参考文献
Grammaticakis
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1952 , vol. 235, p. 546
反应条件
(μ3,η2,η3,η5-acenaphthylene)Ru3(CO)7; 1,1,4,4-tetramethyldisilylethylene in ethylene glycol dimethyl ether T=70°C; 18 h; Inert atmosphere;
参考文献
Hanada, Shiori; Motoyama, Yukihiro; Nagashima, Hideo
European Journal of Organic Chemistry, 2008 , # 24 p. 4097 - 4100
反应条件
1: 95 percent / DMAP / CH2Cl2 2: 97 percent / NaBH4 / ethanol / 20 h View Scheme
参考文献
Ragnarsson, Ulf; Grehn, Leif; Monteiro, Luis S.; Maia, Hernani L. S.
Synlett, 2003 , # 15 p. 2386 - 2388
反应条件
ammonia; oxygen in water
T=150°C; P=22502.3 Torr; 5 h;
参考文献
Nie, Renfeng; Shi, Juanjuan; Xia, Shuixin; Shen, Lian; Chen, Ping; Hou, Zhaoyin; Xiao, Feng-Shou
Journal of Materials Chemistry, 2012 , vol. 22, # 35 p. 18115 - 18118
反应条件
acetaldehyde oxime; NiII chloride hexahydrate; water
8 h; Reflux; chemoselective reaction;
参考文献
Ma, Xiaoyun; He, Ying; Wang, Pengcheng; Lu, Ming
Applied Organometallic Chemistry, 2012 , vol. 26, # 7 p. 377 - 382
反应条件
ammonia; palladium diacetate; di-(1-adamantyl)-n-butylphosphine in 1,4-dioxane
T=100°C; P=1500.15 Torr; 16 h; Autoclave;
参考文献
Wu, Xiao-Feng; Neumann, Helfried; Neumann, Stephan; Beller, Matthias
Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3040 - 3042
反应条件
ammonia
Inert atmosphere;
参考文献
Hanada, Shiori; Motoyama, Yukihiro; Nagashima, Hideo
European Journal of Organic Chemistry, 2008 , # 24 p. 4097 - 4100
反应条件
anhydrous iron chloride; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; hydroxylamine hydrochloride; iodine; potassium carbonate in 1,2-dichloro-ethane
T=90°C; 15 h;
参考文献
Das, Rima; Chakraborty, Debashis
Catalysis Communications, 2012 , vol. 26, p. 48 - 53
