1,2,3,4,5-五碘苯合成路线 (共 6 条)
反应条件
trifluorormethanesulfonic acid; IPy2BF4 in dichloromethane
12 h; Ambient temperature;
参考文献
Barluenga; Gonzalez; Garcia-Martin; Campos
Tetrahedron Letters, 1993 , vol. 34, # 24 p. 3893 - 3896
反应条件
sulfuric acid; iodine; periodic acid
48 h; Ambient temperature; Further byproducts given;
参考文献
Mattern, Daniell Lewis; Chen, Xinhua
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5903 - 5907
反应条件
sulfuric acid; periodic acid; potassium iodide
Ambient temperature; Title compound not separated from byproducts;
参考文献
Mattern, Daniell Lewis
Journal of Organic Chemistry, 1983 , vol. 48, # 24 p. 4772 - 4773
反应条件
(i) Hg(CF3CO2)2, (ii) NaI3; Multistep reaction;
参考文献
Deacon,G.B.; Farquharson,G.J.
Australian Journal of Chemistry, 1977 , vol. 30, p. 1701 - 1713
反应条件
sulfuric acid; iodine; periodic acid
T=55°C; 24 h; other temperature, variation of stoichiometry; Product distributionMechanism;
参考文献
Mattern, Daniell Lewis; Chen, Xinhua
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5903 - 5907
反应条件
sulfuric acid; iodine; periodic acid
48 h; Ambient temperatureother temperature, variation of stoichiometry; Product distributionMechanism;
参考文献
Mattern, Daniell Lewis; Chen, Xinhua
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5903 - 5907