L-(+)-酒石酸二甲酯合成路线 （共 28 条）
反应条件
anhydrous iron chloride; water in acetic acid T=70°C; 3.5 h;
参考文献
Tzschucke, C. Christoph; Pradidphol, Narathip; Dieguez-Vazquez, Alejandro; Kongkathip, Boonsong; Kongkathip, Ngampong; Ley, Steven V.
Synlett, 2008 , # 9 p. 1293 - 1296
反应条件
Dowex® 50W X8 (H+ form) in methanol T=50°C; 22 h; Inert atmosphere;
参考文献
Meier, Bettina; Kollroser, Manfred; Presser, Armin
Monatshefte fur Chemie, 2014 , vol. 145, # 2 p. 305 - 309
反应条件
nickel dichloride 11 h; Heating;
参考文献
Ram, Ram N.; Charles
Tetrahedron, 1997 , vol. 53, # 21 p. 7335 - 7340
反应条件
osmium(VIII) oxide; S,S-(1,3,5-Me3C6H2CH2NHCHPh)2; sodium hydrogensulfite 1.) CH2Cl2, -90 deg C, 2.3 h, 2.) THF, reflux, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 111, p. 9243 - 9244
反应条件
acetyl chloride 6 h; Heating;
参考文献
Kocienski, Philip; Street, Stephen D. A.
Synthetic Communications, 1984 , vol. 14, # 12 p. 1087 - 1092
反应条件
in various solvent(s) T=39°C; 168 h; lipase from Pseudomonas fluorescens;
参考文献
Gutman, Arie L.; Shkolnik, Eleonora; Shapira, Michal
Tetrahedron, 1992 , vol. 48, # 40 p. 8775 - 8780
反应条件
osmium(VIII) oxide; (S,S)-(-)-N,N'-dineohexyl-2,2'-bipyrrolidine; sodium hydrogensulfite 1.) CH2Cl2, -78 deg C, overnight, 3.) THF, water, reflux, 2 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 54, # 25 p. 5834 - 5835
反应条件
methanol-d4 T=20°C; 24 h; regioselective reaction;
参考文献
Dalton Transactions, , # 8 p. 1460 - 1470
反应条件
chloro-trimethyl-silane; 2,2-dimethoxy-propane 24 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 39, # 47 p. 8563 - 8566
参考文献
Journal of the Chemical Society, , vol. 79, p. 282
