1,3-二硝基-2,4,6-三甲基苯合成路线 （共 13 条）
反应条件
1: water; alcohol; ammonium sulfide / 110 - 115 °C 3: concentrated hydrochloric acid / 180 - 200 °C View Scheme
参考文献
Kuester; Stallberg
Justus Liebigs Annalen der Chemie, 1894 , vol. 278, p. 222
反应条件
hydrogenchloride; zinc
参考文献
Kawada, Hiromitsu; Matsunaga, Yoshio; Takamura, Takumi; Terada, Masahiro
Canadian Journal of Chemistry, 1988 , vol. 66, p. 1867 - 1871
反应条件
1: aq. NH3, H2S / ethanol / Heating 2: (i) aq. H2SO4, NaNO2, (ii) (heating) View Scheme
参考文献
Stein,A.R.
Canadian Journal of Chemistry, 1965 , vol. 43, p. 1493 - 1507
反应条件
palladium(IV) oxide; MoO3+Fe2O3 on Al2O3 in 1,2-dichloro-benzene T=210°C; P=228000 Torr;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 29, # 1 p. 117 - 120
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 1 p. 133 - 136
反应条件
nitrogen(IV) oxide; ozone in dichloromethane
T=-10 - 0°C; 1 h;
参考文献
Suzuki, Hitomi; Murashima, Takashi; Kozai, Iku; Mori, Tadashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 14 p. 1591 - 1598
参考文献
Fittig
Justus Liebigs Annalen der Chemie, 1867 , vol. 141, p. 134
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Hofmann,A. W.
Justus Liebigs Annalen der Chemie, 1849 , vol. 71, p. 129
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Dyson; Hunter
Journal of the Society of Chemical Industry, London, 1926 , vol. 45, p. 84 T
Chem. Zentralbl., 1926 , vol. 97, # I p. 3139
Full Text Show Details
Kuester; Stallberg
Justus Liebigs Annalen der Chemie, 1894 , vol. 278, p. 222
反应条件
nitrogen(IV) oxide; ozone; methanesulfonic acid in dichloromethane
T=-10 - 0°C; 9 h;
参考文献
Suzuki, Hitomi; Murashima, Takashi; Kozai, Iku; Mori, Tadashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 14 p. 1591 - 1598
参考文献
Mabery; Hudson
American Chemical Journal, 1901 , vol. 25, p. 260
反应条件
in benzene
Heatingother solvent (neat); Product distributionKineticsRate constant;
参考文献
Oxley, Jimmie C.; Smith, James L.; Ye, Hong; McKenney, Robert L.; Bolduc, Paul R.
Journal of Physical Chemistry, 1995 , vol. 99, # 23 p. 9593 - 9602
参考文献
Mabery; Hudson
American Chemical Journal, 1901 , vol. 25, p. 260
Full Text Show Details
Pictet; Bouvier
Annales de Chimie (Cachan, France), 1918 , vol. <9> 10, p. 263
