三乙氧基-[3-(3-三乙氧基硅烷基丙基硫基)丙基]硅烷合成路线 （共 17 条）
反应条件
sodium hydrogen sulphate; sodium hydrogensulfide; tetrabutylammomium bromide in water
T=75°C; 5.63333 h;
参考文献
Dow Corning Corporation
Patent: US6680398 B1, 2004 ;
Location in patent: Page column 10-11 ;
反应条件
sodium sulfide; sodium hydrogensulfide; tetrabutylammomium bromide in water
T=70 - 82°C; 3 h;
参考文献
Dow Corning Corporation
Patent: US6680398 B1, 2004 ;
Location in patent: Page column 8 ;
反应条件
formic acid in ethanol
参考文献
Krafczyk, Roland; Deschler, Ulrich; Treffeisen, Bjorn
Patent: US2003/23106 A1, 2003 ;
反应条件
formic acid; hydrogen sulfide in ethanol
参考文献
Krafczyk, Roland; Deschler, Ulrich; Treffeisen, Bjorn
Patent: US2003/23106 A1, 2003 ;
反应条件
sodium hydrogensulfide; sodium acetate; tetrabutylammomium bromide in water
参考文献
Dow Corning Corporation
Patent: US6680398 B1, 2004 ;
Location in patent: Page column 11-12 ;
反应条件
sodium sulfide; tetrabutylammomium bromide; sulfur in water
T=80 - 90°C; 5.66667 h; Product distribution / selectivity;
参考文献
Shin-Etsu Chemical Co., Ltd.
Patent: US2006/106240 A1, 2006 ;
Location in patent: Page/Page column 4 ;
反应条件
1: With sulfur in toluene
T=80°C;
2: With tetrabutylammomium bromide; sulfur in water; toluene
T=80 - 85°C; 5.58333 h; Product distribution / selectivity;
参考文献
Shin-Etsu Chemical Co., Ltd.
Patent: US2006/106240 A1, 2006 ;
Location in patent: Page/Page column 4-5 ;
反应条件
1: gamma-mercaptopropyltriethoxysilane With sodium in toluene
T=105°C; 0.5 - 1.36667 h;
2: octanoic acid chloride in toluene
T=20 - 62°C; 1 - 1.58333 h;
3: With water in toluene
T=32 - 50°C; Product distribution / selectivity;
参考文献
General Electric Company
Patent: US6777569 B1, 2004 ;
Location in patent: Page column 6 ;
反应条件
1: With sulfur
T=80°C;
2: With Na2S3; tetrabutylammomium bromide in water
T=80 - 90°C; 3.66667 h; Product distribution / selectivity;
参考文献
Shin-Etsu Chemical Co., Ltd.
Patent: US2006/106240 A1, 2006 ;
Location in patent: Page/Page column 4 ;
反应条件
1: 4,4,13,13-tetraethoxy-3,14-dioxa-8,9-dithia-4,13-disilahexadecane With sodium in toluene
T=110°C; 0.75 - 1.15 h;
2: octanoic acid chloride in toluene
T=45 - 60°C; 1 - 2 h;
3: With water in toluene
T=45°C; Product distribution / selectivity;
参考文献
General Electric Company
Patent: US6777569 B1, 2004 ;
Location in patent: Page column 7-9 ;
