反应条件
1: 1.) NaBH4, BF3*Et2O, 2.) H2O2, aq. NaOH, / 1.) THF, 20 deg C, 1 h, 2.) THF
2: 42 percent / 48percent HBr, H2SO4 / 5 h / 100 °C
3: 1.) EtMgBr / 1.) THF, reflux, 1 h, 2.) THF, 10 min
View Scheme
参考文献
Kawashima, Hidefumi; Yajima, Kazuyoshi; Kuge, Yuji; Hashimoto, Naoto; Miyake, Yoshihiro
Journal of Labelled Compounds and Radiopharmaceuticals, 1997 , vol. 39, # 3 p. 181 - 193
