1,1-二氯-2-硝基乙烯合成路线 （共 8 条）
反应条件
sodium methylate in methanol
参考文献
Frankotte,F. et al.
Bulletin des Societes Chimiques Belges, 1978 , vol. 87, p. 693 - 707
反应条件
sodium methylate in methanol
参考文献
Buevich,V.A. et al.
Journal of Organic Chemistry USSR (English Translation), 1978 , vol. 14, p. 2031 - 2035
Zhurnal Organicheskoi Khimii, 1978 , vol. 14, p. 2197 - 2201
反应条件
in ethanol T=80 - 90°C; 4 h; Heating / reflux; Product distribution / selectivity;
参考文献
Li, Zhong; Qian, Xuhong; Shao, Xusheng; Xu, Xiaoyong; Tian, Zhongzhen; Huang, Qingchun
Patent: US2009/111847 A1, 2009 ;
Location in patent: Page/Page column 6 ;
反应条件
sodium hydroxide in chloroform
参考文献
Takeda Chemical Industries, Ltd.
Patent: US5364989 A1, 1994 ;
反应条件
hydrogenchloride; nitric acid in water
T=20 - 25°C; 3 h;
参考文献
East China University of Science and Technology
Patent: EP1997820 A1, 2008 ;
Location in patent: Page/Page column 9 ;
反应条件
nitrosyl chloride
T=25°C;
参考文献
Jakubowitsch; Lemke
Zhurnal Obshchei Khimii, 1949 , vol. 19, p. 657
Chem.Abstr., 1950 , p. 1011
反应条件
iron(III) chloride; nitrosyl chloride
T=0°C;
参考文献
Nesmejanow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1958 , p. 841,844;engl.Ausg.S.819,822
参考文献
Nesmejanow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1958 , p. 841,844;engl.Ausg.S.819,822
