1,3,3-三苯基-1-丙酮合成路线 (共 136 条)
反应条件
1: 65 percent / 4-toluenesulfonic acid / 100 °C 2: 8 percent / hexane / 2 h / Ambient temperature; Irradiation View Scheme
参考文献
Monatshefte fuer Chemie, , vol. 124, p. 209 - 216
反应条件
1: 65 percent / 4-toluenesulfonic acid / 100 °C 2: 38 percent / hexane / 2 h / Ambient temperature; Irradiation View Scheme
参考文献
Algarra, Felipe; Baldovi, Maria V.; Garcia, Hermenegildo; Miranda, Miguel A.; Primo, Jaime
Monatshefte fuer Chemie, 1993 , vol. 124, p. 209 - 216
反应条件
chloroform; caesium carbonate; triphenylphosphine; palladium diacetate in toluene
T=80°C; 24 h;
参考文献
Tang, Yi-Qiang; Lv, Huan; He, Xiao-Na; Lu, Jian-Mei; Shao, Li-Xiong
Catalysis Letters, 2011 , vol. 141, # 5 p. 705 - 708
反应条件
AlCl3, aluminium chloride in benzene
T=30°C; Friedel-Crafts Acylation; 3.63333 h; Temperature;
参考文献
Zhou, Yang; Li, Xinyao; Hou, Shili; Xu, Jiaxi
Journal of Molecular Catalysis A: Chemical, 2012 , vol. 365, p. 203 - 211
反应条件
anhydrous iron chloride; silver hexafluoroantimonate in 1,2-dichloro-ethane
T=80°C; 24 h;
参考文献
Jefferies, Latisha R.; Cook, Silas P.
Tetrahedron, 2014 , vol. 70, # 27-28 p. 4204 - 4207
反应条件
(Z,Z)-1,5-cyclooctadiene; rhodium-grafted hydrotalcite in 1,4-dioxane
T=150°C; 24 h;
参考文献
Yamamoto, Tetsuya; Iizuka, Michiko; Takenaka, Hiroto; Ohta, Tetsuo; Ito, Yoshihiko
Journal of Organometallic Chemistry, 2009 , vol. 694, # 9-10 p. 1325 - 1332
反应条件
chloro-trimethyl-silane; [Rh(η6-C6H5F){PCyp2(η2-C5H7)}][BArF4] in tetrahydrofuran
T=20°C; 2 h;
参考文献
Douglas, Thomas M.; Notre, Jerome Le; Brayshaw, Simon K.; Frost, Christopher G.; Weller, Andrew S.
Chemical Communications, 2006 , # 32 p. 3408 - 3410
反应条件
sodium acetate; antimony trichloride; palladium diacetate in acetic acid
T=25°C; 24 h;
参考文献
Cho, Chan Sik; Motofusa, Shin-ichi; Ohe, Kouichi; Uemura, Sakae; Shim, Sang Chul
Journal of Organic Chemistry, 1995 , vol. 60, # 4 p. 883 - 888
反应条件
water; [Rh(NCMe)2(cod)][BF4] in tetrahydrofuran
T=60°C; 2 h;
参考文献
Oi, Shuichi; Moro, Mitsutoshi; Ito, Hisanori; Honma, Yoshio; Miyano, Sotaro; Inoue, Yoshio
Tetrahedron, 2002 , vol. 58, # 1 p. 91 - 97
反应条件
tetrabutyl ammonium fluoride; antimony trichloride; acetic acid; palladium diacetate in acetonitrile
T=60°C; 28 h;
参考文献
Denmark, Scott E.; Amishiro, Nobuyoshi
Journal of Organic Chemistry, 2003 , vol. 68, # 18 p. 6997 - 7003