反应条件
in carbon disulfide
stirring for 2 h; vol. reduction (vac.), hexane addn., crystn. (-50°C), decantation(-50°C, absence of moisture), drying (vac., <=20°C);
参考文献
Steudel, Ralf; Bergemann, Klaus; Buschmann, Juergen; Luger, Peter
Inorganic Chemistry, 1996 , vol. 35, # 8 p. 2184 - 2188
