1-苯基-3-丁烯-2-醇合成路线 （共 9 条）
反应条件
sodium hydride in tetrahydrofuran T=-3°C; 3 h;
参考文献
Mulzer, Johann; Steffen, Ulrich; Martin, Harry J.; Zorn, Ludwig
European Journal of Organic Chemistry, 2005 , # 6 p. 1028 - 1043
反应条件
isopropyl alcohol; [{RuCl(μ-Cl)(η6-C6Me6)}2] T=82°C; 22 h;
参考文献
Cadierno, Victorio; Francos, Javier; Gimeno, Jose; Nebra, Noel
Chemical Communications, 2007 , # 24 p. 2536 - 2538
反应条件
dichloro(.eta.3:.eta.2:.eta.3-dodeca-2,6,10-triene-1,12-diyl)ruthenium(IV); water; sodium formate T=100°C; 20 h; Inert atmosphere;
参考文献
Cadierno, Victorio; Crochet, Pascale; Francos, Javier; Garcia-Garrido, Sergio E.; Gimeno, Jose; Nebra, Noel
Green Chemistry, 2009 , vol. 11, # 12 p. 1992 - 2000
反应条件
bis(tricyclohexylphosphine)benzylidene ruthenium(IV) dichloride in toluene 2 h; Heating;
参考文献
Gurjar, Mukund K.; Yakambram, Pedduri
Tetrahedron Letters, 2001 , vol. 42, # 21 p. 3633 - 3636
反应条件
dichloro(.eta.3:.eta.2:.eta.3-dodeca-2,6,10-triene-1,12-diyl)ruthenium(IV); water; sodium formate T=100°C; 20 h; Inert atmosphere;
参考文献
Cadierno, Victorio; Crochet, Pascale; Francos, Javier; Garcia-Garrido, Sergio E.; Gimeno, Jose; Nebra, Noel
Green Chemistry, 2009 , vol. 11, # 12 p. 1992 - 2000
反应条件
1: 1) SOCl2 / 1) Et2O, RT, 12 h, 2) THF, -78 deg C, 3 h
2: 90 percent / Me3Al / hexane; CH2Cl2 / 16 h / Ambient temperature
View Scheme
参考文献
Fleming; Sanderson; Terrett
Synthesis, 1992 , # 1-2 p. 69 - 74
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in ethyl acetate
Reflux;
参考文献
Shen, Zhi-Liang; Goh, Kelvin Kau Kiat; Cheong, Hao-Lun; Wong, Colin Hong An; Lai, Yin-Chang; Yang, Yong-Sheng; Loh, Teck-Peng
Journal of the American Chemical Society, 2010 , vol. 132, # 45 p. 15852 - 15855
反应条件
Grubb's 2nd generation catalyst; phenol in toluene
T=110°C; 0.5 h; Inert atmosphere;
参考文献
Schmidt, Bernd; Hauke, Sylvia
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 25 p. 4194 - 4206
反应条件
acetyl chloride in ethanol
T=23°C; 1 h; Title compound not separated from byproducts;
参考文献
Yadav, Veejendra K.; Ganesh Babu
Tetrahedron, 2003 , vol. 59, # 46 p. 9111 - 9116
