吲哚并[2,3-A]咔唑合成路线 (共 14 条)
反应条件
1: With sulfuric acid in ethanol T=65°C; Inert atmosphere; 2: With acetic acid; trifluoroacetic acid T=100°C; 15 h;
参考文献
Nippon Steel Chemical Co., Ltd.
Patent: EP2166011 A1, 2010 ;
Location in patent: Page/Page column 20 ;
反应条件
1: With sulfuric acid in ethanol T=20 - 65°C; 4.08 h; Inert atmosphere; 2: With acetic acid; trifluoroacetic acid T=100°C; 15 h;
参考文献
Nippon Steel Chemical Co., Ltd.
Patent: EP2415772 A1, 2012 ;
Location in patent: Page/Page column 33-34 ;
反应条件
trifluoroacetic acid in acetic acid T=100°C; Fischer indole synthesis;
参考文献
Hu, Yong-Zhou; Chen, You-Qin
Synlett, 2005 , # 1 art. no. U25804ST, p. 42 - 48
反应条件
trifluoroacetic acid in acetic acid Fischer indole synthesis; 12 h; Heating;
参考文献
Hu, Yong-Zhou; Chen, You-Qin
Synlett, 2005 , # 1 art. no. U25804ST, p. 42 - 48
反应条件
hydrazine in tetrahydrofuran Heating;
参考文献
Banerji, Avijit; Bandyopadhyay, Debasish; Basak, Bidyut; Biswas, Pizush Kanti; Banerji, Julie; Chatterjee, Asima
Bulletin of the Chemical Society of Japan, 2007 , vol. 80, # 6 p. 1199 - 1201
反应条件
acetic acid Heating;
参考文献
Curiel, David; Cowley, Andrew; Beer, Paul D.
Chemical Communications, 2005 , # 2 p. 236 - 238
反应条件
in acetic acid; trifluoroacetic acid 12 h; Heating;
参考文献
Royer, Herve; Joseph, Delphine; Prim, Damien; Kirsch, Gilbert
Synthetic Communications, 1998 , vol. 28, # 7 p. 1239 - 1251
反应条件
acetic acid Fischer Indole Synthesis; 40 h; Reflux; Overall yield = 97.9percent;
参考文献
Journal of Organic Chemistry, , vol. 78, # 16 p. 7796 - 7808
反应条件
hydrogenchloride; sodium tetrahydroborate Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Heterocycles, , vol. 45, # 9 p. 1647 - 1650
反应条件
acetic acid anschliessendes Erhitzen mit konz. wss. HCl;
参考文献
Chemistry and Industry (London, United Kingdom), , p. 363