7h-苯并(c)芴-7-酮合成路线 (共 34 条)
反应条件
hydrogen; palladium on activated charcoal in tetrahydrofuran Ambient temperature;
参考文献
Alt, Helmut G.; Zenk, Roland; Milius, Wolfgang
Journal of Organometallic Chemistry, 1996 , vol. 514, # 1-2 p. 257 - 270
反应条件
aluminium trichloride; sodium chloride T=145°C;
参考文献
Baddar
Journal of the Chemical Society, 1941 , p. 310
参考文献
Baddar
Journal of the Chemical Society, 1941 , p. 310
反应条件
CsO2CCMe3; [Pd(P{(C6H11)3})2] in N,N-dimethyl-formamide
T=110°C; Carbonylation; cyclization; P=760.051 Torr; 7 h;
参考文献
Campo, Marino A.; Larock, Richard C.
Journal of Organic Chemistry, 2002 , vol. 67, # 16 p. 5616 - 5620
反应条件
lithium diisopropyl amide in tetrahydrofuran; cyclohexane
T=-78 - 20°C;
参考文献
Tosoh Corporation
Patent: EP2006278 A2, 2008 ;
Location in patent: Page/Page column 26; 27 ;
反应条件
in N,N-dimethyl-formamide
T=130°C; 16 h; Reagent/catalystSolvent;
参考文献
Zheng, Shuyan; Tan, Hongsheng; Zhang, Xiaoguang; Yu, Chunhui; Shen, Zhengwu
Tetrahedron Letters, 2014 , vol. 55, # 5 p. 975 - 978
反应条件
air; graphene-supported KOH composite in N,N-dimethyl-formamide
T=20°C; 24 h;
参考文献
Zhang, Xin; Ji, Xuan; Su, Ruifei; Weeks, Brandon L.; Zhang, Zhao; Deng, Songlu
ChemPlusChem, 2013 , vol. 78, # 7 p. 703 - 711
反应条件
cesium fluoride; tris-(o-tolyl)phosphine; bis(dibenzylideneacetone)-palladium(0) in toluene; acetonitrile
T=110°C; 12 h;
参考文献
Zhang, Xiaoxia; Larock, Richard C.
Organic Letters, 2005 , vol. 7, # 18 p. 3973 - 3976
Title/Abstract Full Text View citing articles Show Details
Waldo, Jesse P.; Zhang, Xiaoxia; Shi, Feng; Larock, Richard C.
Journal of Organic Chemistry, 2008 , vol. 73, # 17 p. 6679 - 6685
反应条件
tert.-butylhydroperoxide; biscyclopentadienyliron(II) in decane; acetonitrile
T=20 - 90°C; 24 h;
参考文献
Wertz, Sebastian; Leifert, Dirk; Studer, Armido
Organic Letters, 2013 , vol. 15, # 4 p. 928 - 931
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; trimethylacetic anhydride; 1,2-bis-(diphenylphosphino)ethane; potassium iodide
T=160°C; 0.5 h; Inert atmosphereMicrowave irradiationSealed tube; Wavelength;
参考文献
Fukuyama, Takahide; Maetani, Shinji; Miyagawa, Kazusa; Ryu, Ilhyong
Organic Letters, 2014 , vol. 16, # 12 p. 3216 - 3219