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diazadiene palladium in toluene

samarium; mercury dichloride in tetrahydrofuran T=-78 - 20°C;

methanol; sulfuric acid; mercury(II) oxide

1: Al(OiPr)3 2: (i) polyphosphoric acid, (ii) H2, Raney-Ni View Scheme

sodium hydrogen sulphate; hydroquinone in tetrahydrofuran T=120°C; P=30 Torr; Inert atmosphere;

1.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere; Cooling with acetone-dry ice 1.2: -78 - 4 °C / Inert atmosphere 2.1: tris-(dibenzylideneacetone)dipalladium(0); [(R)-methoxy(furyl)BIPHEP]; cesium fluoride / tetrahydrofuran / 12 h / 60 °C / Inert atmosphere View Scheme