2,3-二甲氧基-5-甲基-1,4-苯醌合成路线 （共 103 条）
反应条件
1: CuBr / dimethylformamide; H2O / 130 °C 2: O2 / Co(salen) View Scheme
参考文献
Tetrahedron Letters, , vol. 46, # 8 p. 1255 - 1257
反应条件
1: 100 percent / MCPA; p-TsOH / CHCl3 / 3 h / 50 °C 2: Na / methanol / 20 °C 3: CuBr / dimethylformamide; H2O / 130 °C 4: O2 / Co(salen) View Scheme
参考文献
Tetrahedron Letters, , vol. 46, # 8 p. 1255 - 1257
反应条件
1: Na / methanol / 20 °C 2: CuBr / dimethylformamide; H2O / 130 °C 3: O2 / Co(salen) View Scheme
参考文献
Tetrahedron Letters, , vol. 46, # 8 p. 1255 - 1257
反应条件
1: 82 percent / molecular sieves 4 Angstroem / Amberlite IR 120-plus / benzene / Heating 2: K2CO3 / Bu4NHSO4 / acetone / 24 h / Heating 3: TsOH / methanol; H2O / 16 h / Ambient temperature 4: 91 percent / K2CO3 / acetone / 15 h / Heating 5: 96 percent / H2 / 10percent Pd/C / tetrahydrofuran / 6 h / Ambient temperature 6: 92 percent / K2(SO3)2NO, KH2SO4 / benzene; H2O / 3 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 8 p. 797 - 802
反应条件
1: 97 percent / H2 / 10percent Pd/C / acetic acid / 72 h / 30002.4 Torr / Ambient temperature 2: 96 percent / 57percent HI, 30percent aq. H3PO2 / Heating 3: 82 percent / molecular sieves 4 Angstroem / Amberlite IR 120-plus / benzene / Heating 4: K2CO3 / Bu4NHSO4 / acetone / 24 h / Heating 5: TsOH / methanol; H2O / 16 h / Ambient temperature 6: 91 percent / K2CO3 / acetone / 15 h / Heating 7: 96 percent / H2 / 10percent Pd/C / tetrahydrofuran / 6 h / Ambient temperature 8: 92 percent / K2(SO3)2NO, KH2SO4 / benzene; H2O / 3 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 8 p. 797 - 802
反应条件
1: K2CO3 / Bu4NHSO4 / acetone / 24 h / Heating 2: TsOH / methanol; H2O / 16 h / Ambient temperature 3: 91 percent / K2CO3 / acetone / 15 h / Heating 4: 96 percent / H2 / 10percent Pd/C / tetrahydrofuran / 6 h / Ambient temperature 5: 92 percent / K2(SO3)2NO, KH2SO4 / benzene; H2O / 3 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 8 p. 797 - 802
反应条件
1: 91 percent / K2CO3 / acetone / 15 h / Heating 2: 96 percent / H2 / 10percent Pd/C / tetrahydrofuran / 6 h / Ambient temperature 3: 92 percent / K2(SO3)2NO, KH2SO4 / benzene; H2O / 3 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 8 p. 797 - 802
反应条件
1: 96 percent / H2 / 10percent Pd/C / tetrahydrofuran / 6 h / Ambient temperature 2: 92 percent / K2(SO3)2NO, KH2SO4 / benzene; H2O / 3 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 8 p. 797 - 802
反应条件
1: TsOH / methanol; H2O / 16 h / Ambient temperature 2: 91 percent / K2CO3 / acetone / 15 h / Heating 3: 96 percent / H2 / 10percent Pd/C / tetrahydrofuran / 6 h / Ambient temperature 4: 92 percent / K2(SO3)2NO, KH2SO4 / benzene; H2O / 3 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 8 p. 797 - 802
反应条件
in para-xylene thermolysis; 0.333333 h; Heating;
参考文献
Boullais, Claude; Rannou, Christelle; Reveillere, Emmanuel; Mioskowski, Charles
European Journal of Organic Chemistry, 2000 , # 5 p. 723 - 727
