2,3-二甲氧基-5-甲基-1,4-苯醌合成路线 （共 103 条）
反应条件
1: With dihydrogen peroxide; toluene-4-sulfonic acid; acetic acid T=75°C; 0.5 h; 2: With nitric acid in water T=0 - 5°C; 0.00833333 h;
参考文献
Occhipinti, Giovanni; Liguori, Lucia; Tsoukala, Anna; Bjorsvik, Hans-Rene
Organic Process Research and Development, 2010 , vol. 14, # 6 p. 1379 - 1384
反应条件
titanium superoxide; dihydrogen peroxide; acetic acid in water T=50°C; 2 h;
参考文献
Dewkar, Gajanan K.; Shaikh, Tanveer M.; Pardhy; Kulkarni, Swati S.; Sudalai, Arumugam
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 7 p. 1530 - 1532
反应条件
iron(III) chloride in water; benzene 3 h; Ambient temperature;
参考文献
Minami, Norio; Kijima, Shizumasa
Chemical & Pharmaceutical Bulletin, 1980 , vol. 28, # 5 p. 1648 - 1650
反应条件
dihydrogen peroxide in formic acid; water T=40°C; 2 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 5 p. 1652 - 1657
反应条件
(i) ZnCl2, Et2O, (ii) MnO2, PE; Multistep reaction;
参考文献
Angewandte Chemie, , vol. 79, p. 979 - 980
反应条件
pyridine-2,6-dicarboxylic acid; ammonium cerium(IV) nitrate in water; acetonitrile a.) 20 min, 0 deg C b.) 10 min, RT;
参考文献
Keinan, Ehud; Eren, Doron
Journal of Organic Chemistry, 1987 , vol. 52, # 17 p. 3872 - 3875
反应条件
sulfuric acid; 3,3-dimethyldioxirane in acetone T=20°C; 2 h;
参考文献
Synthesis, , # 6 p. 560 - 562
反应条件
1: 86.4 percent / 99 percent N2H4*H2O / methanol / 5 h / Heating 2: 85 percent / K3Fe(CN)6; 25 percent NH4OH / H2O; CH2Cl2 / 4 h / 20 °C 3: 65 percent / Zn-Hg / acetic acid; toluene; H2O / 0.75 h / Heating 4: 80 percent / 50 percent H2O2; 98 percent HCOOH; phosphomolybdic acid / 0.25 h / 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 31, # 5 p. 657 - 660
反应条件
1: 70.6 percent / AlCl3 / diethyl ether / 72 h / Ambient temperature 2: 72.3 percent / Zn-Hg, conc. HCl / H2O; toluene / 14 h / Heating 3: 1.3 g / ON(SO3K)2, sodium acetate / acetone; H2O / 2 h / Ambient temperature View Scheme
参考文献
Chemical and pharmaceutical bulletin, , vol. 30, # 8 p. 2797 - 2819
反应条件
in toluene T=170°C; 7 h;
参考文献
Ruttimann; Lorenz
Helvetica Chimica Acta, 1990 , vol. 73, # 4 p. 790 - 796
