2-乙酰基-3-氧代辛酸乙酯合成路线 （共 8 条）
反应条件
1: sodium ethylate; ethanol 2: sodium ethylate; ethanol; benzene 3: aq.-ethanolic sulfuric acid View Scheme
参考文献
Nakazawa; Matsuura
Yakugaku Zasshi, 1952 , vol. 72, p. 51,53
Chem.Abstr., 1952 , p. 11142
反应条件
1: sodium ethylate; ethanol 2: sodium ethylate; ethanol; benzene 3: aq.-ethanolic sulfuric acid 4: sodium; sodium ethylate; xylene View Scheme
参考文献
Nakazawa; Matsuura
Yakugaku Zasshi, 1952 , vol. 72, p. 51,53
Chem.Abstr., 1952 , p. 11142
反应条件
1: ethyl acetoacetate With ethanol; magnesium in tetrachloromethane; toluene
1 h; Heating;
2: n-pentylcarbonyl chloride in tetrachloromethane; toluene
T=0 - 20°C; 1.5 h;
参考文献
Jung, Jae-Chul; Blake Watkins; Avery, Mitchell A.
Heterocycles, 2005 , vol. 65, # 1 p. 77 - 94
反应条件
ethanol; magnesium diethoxide; benzene
Anschliessend Behandeln mit Hexanoylchlorid.;
参考文献
Nakazawa; Matsuura
Yakugaku Zasshi, 1952 , vol. 72, p. 51,53
Chem.Abstr., 1952 , p. 11142
参考文献
Locquin
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1902 , vol. 135, p. 110
Bulletin de la Societe Chimique de France, 1904 , vol. <3> 31, p. 593,761
Full Text Show Details
Bouveault; Bongert
Bulletin de la Societe Chimique de France, 1902 , vol. <3> 27, p. 1044,1049
反应条件
ethanol; sodium ethanolate
参考文献
Nakazawa; Matsuura
Yakugaku Zasshi, 1952 , vol. 72, p. 51,53
Chem.Abstr., 1952 , p. 11142
反应条件
sodium chloride in water; dimethyl sulfoxide
Krapcho decarbethoxylation; 12 h; Heating;
参考文献
Krueckert, Karsten; Flachsbarth, Birte; Schulz, Stefan; Hentschel, Ute; Weldon, Paul J.
Journal of Natural Products, 2006 , vol. 69, # 6 p. 863 - 870
反应条件
1: sodium ethylate; ethanol
2: sodium ethylate; ethanol; benzene
3: aqueous hydrochloric acid
View Scheme
参考文献
Nakazawa; Matsuura
Yakugaku Zasshi, 1952 , vol. 72, p. 51,53
Chem.Abstr., 1952 , p. 11142
