2-[(氯乙酰基)氨基]-4,5,6,7-四氢-1-苯并噻吩-3-羧酸乙酯合成路线 （共 8 条）
反应条件
in acetic acid T=20°C; 2 h;
参考文献
Assy, Mohamed G.; Sherif, Mohamed H.; Amr, Abd El-Galil E.; Abdelsalam, Osama I.; Al-Omar, Mohamed A.; Abdalla, Mohamed M.; Ragab, Islam
Journal of Heterocyclic Chemistry, 2013 , vol. 50, # 4 p. 766 - 773
反应条件
1: sulphur, diethylamine / ethanol / 50 °C 2: 63 percent / acetic acid / 3 h / Heating View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 33, p. 298 - 301
反应条件
1: sulfur; n-ethyl morpholine / ethanol / 3 h / 20 °C 2: chloroform / 3 h / |Reflux View Scheme
参考文献
Bioconjugate Chemistry, , vol. 23, # 12 p. 2403 - 2416
反应条件
1: sulfur; n-ethyl morpholine / ethanol / 3 h / 20 °C 2: chloroform / 3 h / |Reflux View Scheme
参考文献
Bioconjugate Chemistry, , vol. 23, # 12 p. 2403 - 2416
反应条件
1: 50.9 percent / K2Cr2O7 / aq. acetic acid
2: KOH / methanol / 1 h / 20 °C
View Scheme
参考文献
Kharizomenova, I. A.; Kapustina, M. V.; Grinev, A. N.; Sheinker, Yu. N.; Alekseeva, L. M.; Kuleshova, E. F.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1984 , vol. 20, # 12 p. 1339 - 1342
Khimiya Geterotsiklicheskikh Soedinenii, 1984 , # 12 p. 1626 - 1629
反应条件
1: 50.9 percent / K2Cr2O7 / aq. acetic acid
2: KOH / methanol / 1 h / 20 °C
3: 1. NaNO2, conc. HCl; 2. copper acetate / 1. dioxane, -7 to -10 deg C, 20 min; 2. dioxane, ethanol, 70 deg C, 30 min
4: 45.9 percent / NaOH; aq. HCl / ethanol / 0.33 h / Heating
View Scheme
参考文献
Kharizomenova, I. A.; Kapustina, M. V.; Grinev, A. N.; Sheinker, Yu. N.; Alekseeva, L. M.; Kuleshova, E. F.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1984 , vol. 20, # 12 p. 1339 - 1342
Khimiya Geterotsiklicheskikh Soedinenii, 1984 , # 12 p. 1626 - 1629
反应条件
in 1,4-dioxane
4 h; Heating;
参考文献
Gadad, A K; Kumar, Hemant; Shishoo, C J; Khazi, I M; Mahajanshetti, C S
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1994 , vol. 33, p. 298 - 301
参考文献
Gadad, A K; Kumar, Hemant; Shishoo, C J; Khazi, I M; Mahajanshetti, C S
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1994 , vol. 33, p. 298 - 301
