5-氯-1-甲基-1H-吲哚-2,3-二酮合成路线 （共 20 条）
反应条件
CaH2 in N,N-dimethyl-formamide T=100°C; 4 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 45, # 4 p. 969 - 973
反应条件
copper(l) iodide; oxygen; 2,2,2-trimethylacetic acid in dimethyl sulfoxide T=130°C; 23 h;
参考文献
European Journal of Organic Chemistry, , vol. 2014, # 14 p. 2878 - 2882
反应条件
oxygen; copper dichloride in tetrahydrofuran T=100°C; P=760.051 Torr; 20 h;
参考文献
Journal of the American Chemical Society, , vol. 132, # 26 p. 8900 - 8902
反应条件
ammonium cerium(IV) nitrate in water; acetonitrile T=20°C; 15 h;
参考文献
Chemistry - A European Journal, , vol. 13, # 4 p. 1032 - 1046
反应条件
trichloroisocyanuric acid; sulfuric acid
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 42 p. 7372 - 7386
反应条件
1,4-diaza-bicyclo[2.2.2]octane in chloroform Friedel-Crafts acylation; 22 h; Heating;
参考文献
Synthesis, , # 6 p. 904 - 908
反应条件
sodium hydroxide; water
参考文献
Gazzetta Chimica Italiana, , vol. 85, p. 840,841
反应条件
air in chloroform Cyclization; 18 h; Heating;
参考文献
Tetrahedron Letters, , vol. 41, # 18 p. 3475 - 3478
反应条件
1: NH2OH*HCl; Na2SO4; aq. conc. HCl / Heating 2: H2SO4 / 80 °C 3: NaH / N,N-dimethyl-acetamide / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 12, # 17 p. 2427 - 2430
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / N,N-dimethyl-formamide / 20 °C / |Inert atmosphere 2: potassium carbonate / methanol / 2.5 h / 20 °C 3: hydrogenchloride; water / methanol / 12 h / 50 °C 4: copper(l) iodide; 2,2,2-trimethylacetic acid; oxygen / dimethyl sulfoxide / 23 h / 130 °C View Scheme
参考文献
European Journal of Organic Chemistry, , vol. 2014, # 14 p. 2878 - 2882
