1: 2-(2-nitrophenyl)-1H-benzo[d]imidazole With sodium hydride in tetrahydrofuran
T=0 - 20°C; 1 h;
2: methyl iodide in tetrahydrofuran
T=20°C;
参考文献
Das, T. Mohan; Rao, Chebrolu P.; Kalle, Nattinen; Rissanen, Kari
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 3 p. 661 - 665
benzylidene malonitrile in ethanol
12 h; Ambient temperature;
参考文献
Chikashita, Hidenori; Nishida, Shuichi; Miyazaki, Makoto; Morita, Yasuhiro; Itoh, Kazuyoshi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 737 - 746
1: 85 percent / methanol / 0.08 h / Ambient temperature
2: 92 percent / methanol / 6 h / Ambient temperature
3: 97 percent / benzylidenemalonitrile / ethanol / 12 h / Ambient temperature
View Scheme
参考文献
Chikashita, Hidenori; Nishida, Shuichi; Miyazaki, Makoto; Morita, Yasuhiro; Itoh, Kazuyoshi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 737 - 746
1: 92 percent / methanol / 6 h / Ambient temperature
2: 97 percent / benzylidenemalonitrile / ethanol / 12 h / Ambient temperature
View Scheme
参考文献
Chikashita, Hidenori; Nishida, Shuichi; Miyazaki, Makoto; Morita, Yasuhiro; Itoh, Kazuyoshi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 737 - 746
1: 85 percent / methanol / 0.08 h / Ambient temperature
2: 92 percent / methanol / 6 h / Ambient temperature
3: 97 percent / benzylidenemalonitrile / ethanol / 12 h / Ambient temperature
View Scheme
参考文献
Chikashita, Hidenori; Nishida, Shuichi; Miyazaki, Makoto; Morita, Yasuhiro; Itoh, Kazuyoshi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 737 - 746
1.1: AcOH; Cu(OAc)2*H2O / methanol; H2O / 3 h / Heating
1.2: 72 percent / Na2S; aq. HCl / 1 h / Heating
2.1: NaH / tetrahydrofuran / 1 h / 0 - 20 °C
2.2: 85 percent / tetrahydrofuran / 20 °C
View Scheme
参考文献
Das, T. Mohan; Rao, Chebrolu P.; Kalle, Nattinen; Rissanen, Kari
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 3 p. 661 - 665
Hawkins, David; Lindley, John M.; McRobbie, Ian M.; Meth-Cohn, Otto
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2387 - 2391
Hawkins, David; Lindley, John M.; McRobbie, Ian M.; Meth-Cohn, Otto
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2387 - 2391
