β-D-葡萄糖五乙酸酯合成路线 （共 318 条）
反应条件
1: zinc chloride 2: sodium methylate; methanol View Scheme
参考文献
Kariyone et al.
Yakugaku Zasshi, 1952 , vol. 72, p. 13
Chem.Abstr., 1952 , p. 11114
反应条件
1: 78 percent / tin(IV) chloride / CH2Cl2 / 24 h / 20 °C 2: 99 percent / K2CO3 / tetrahydrofuran; methanol / 5 h / 20 °C View Scheme
参考文献
Nicolaou; Winssinger; Pastor; DeRoose
Journal of the American Chemical Society, 1997 , vol. 119, # 2 p. 449 - 450
反应条件
sodium methylate; tin(IV) chloride 1.) PhH, 60 deg C; 2.) MeOH, 25 deg C; Yield given. Multistep reaction;
参考文献
Nicolaou, K. C.; Randall, J. L.; Furst, G. T.
Journal of the American Chemical Society, 1985 , vol. 107, # 19 p. 5556 - 5558
反应条件
1: 78 percent / tin(IV) chloride / CH2Cl2 / 24 h / 20 °C 2: 99 percent / K2CO3 / tetrahydrofuran; methanol / 5 h / 20 °C View Scheme
参考文献
Nicolaou; Winssinger; Pastor; DeRoose
Journal of the American Chemical Society, 1997 , vol. 119, # 2 p. 449 - 450
反应条件
sodium methylate; tin(IV) chloride 1.) PhH, 60 deg C; 2.) MeOH, 25 deg C; Yield given. Multistep reaction;
参考文献
Nicolaou, K. C.; Randall, J. L.; Furst, G. T.
Journal of the American Chemical Society, 1985 , vol. 107, # 19 p. 5556 - 5558
反应条件
1: toluene-4-sulfonic acid 2: sodium methylate; methanol View Scheme
参考文献
Cohen et al.
Journal of Biological Chemistry, 1952 , vol. 195, p. 607,608
反应条件
1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / |Inert atmosphere 2: methanol; sodium methylate / 20 °C / pH 10 - 11 View Scheme
参考文献
Wei, Jinhua; Lv, Xun; Lue, Yang; Yang, Gangzhu; Fu, Lifeng; Yang, Liu; Wang, Jianjun; Gao, Jianhui; Cheng, Shuihong; Duan, Qian; Jin, Cheng; Li, Xuebing
European Journal of Organic Chemistry, 2013 , # 12 p. 2414 - 2419
反应条件
Yield given. Multistep reaction;
参考文献
Carbohydrate Research, , vol. 117, p. 89 - 94
反应条件
1: 25 percent / molecular sieves 4 Angstroem; BF3*Et2O / CH2Cl2 / 48 h / 40 °C 2: 93 percent / sodium methoxide / methanol / 0.25 h / 20 °C View Scheme
参考文献
Kroeger, Lars; Thiem, Joachim
Journal of Carbohydrate Chemistry, 2003 , vol. 22, # 1 p. 9 - 24
反应条件
1: 100 percent / 30percent HBr in AcOH / CH2Cl2 / Ambient temperature 2: Ag2CO3 / 4A molecular sieves / CH2Cl2 / 60 h / Ambient temperature 3: K2CO3 / methanol / 4.5 h / Ambient temperature 4: NaH / dimethylformamide / 8 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 52, # 22 p. 7663 - 7678
