β-D-葡萄糖五乙酸酯合成路线 （共 318 条）
反应条件
1-ethyl-3-methyl-imidazolium benzoate T=20°C; 4 h;
参考文献
Synlett, , # 9 SPEC. ISS. p. 1283 - 1286
反应条件
1: acetic anhydride With sodium acetate 0.333333 h; RefluxInert atmosphere; 2: D-glucopyranose HeatingInert atmosphere;
参考文献
Synthesis, , # 19 art. no. C03810SS, p. 3248 - 3258
反应条件
potassium acetate T=135°C; Acetylation; 0.25 h;
参考文献
Journal of Carbohydrate Chemistry, , vol. 16, # 3 p. 327 - 342
反应条件
acetic anhydride; sodium acetate in xylene T=90 - 105°C; 17 h;
参考文献
EP1544207 A1, ;
Page/Page column 10 ;
反应条件
sodium isothiocyanate
参考文献
Bulletin of the Chemical Society of Japan, , vol. 4, p. 21
反应条件
potassium fluoride; 4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane in acetonitrile T=80°C; 0.166667 h; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 7, # 3 p. 564 - 575
反应条件
sulfuric acid; acetic acid T=0 - 20°C; 72 h;
参考文献
Tetrahedron, , vol. 70, # 7 p. 1492 - 1496
反应条件
in pyridine T=0 - 20°C; Acetylation;
参考文献
Tetrahedron, , vol. 54, # 32 p. 9489 - 9506
反应条件
1: 84 percent / HgO, HgBr2, CaSO4 / CHCl3 / 48 h / Ambient temperature 2: 90 percent / CH3ONa / methanol / 3 h 3: 86 percent / KOH / 130 °C 4: 93 percent / CF3COOH / CH2Cl2 / 0.5 h / 0 °C 5: oxalyl chloride, DMF / CH2Cl2 / 0.5 h 6: 52 percent / Et4NBr, molecular sieves 4A, DMF / CH2Cl2 / 72 h / Heating 7: H2 / 10percent Pd/C / acetic acid / 760 Torr 8: pyridine 9: BF3*Et2O / toluene / 6 h / 55 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 53, # 24 p. 5629 - 5647
反应条件
triethylsilyl trifluoromethanesulphonate T=0°C; 0.0833333 h;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 14 p. 969 - 970
