1: With oxygen; methylene blue in hexane; isopropyl alcohol T=4°C; Oxidation; 5 h; Irradiation; 2: With potassium iodide in ethanol T=20°C; Reduction; 1 h; 3: With potassium hydroxide in methanol T=90°C; Hydrolysis; 1 h; Title compound not separated from byproducts;
参考文献
El Hafidi; Michel; Bascoul; Crastes De Paulet
Chemistry and Physics of Lipids, 1999 , vol. 100, # 1-2 p. 127 - 138
1: With oxygen; methylene blue in hexane; isopropyl alcohol T=4°C; Oxidation; 5 h; Irradiation; 2: With potassium iodide in ethanol T=20°C; Reduction; 1 h; Title compound not separated from byproducts;
参考文献
El Hafidi; Michel; Bascoul; Crastes De Paulet
Chemistry and Physics of Lipids, 1999 , vol. 100, # 1-2 p. 127 - 138
1: With oxygen; methylene blue in hexane; isopropyl alcohol T=4°C; Oxidation; 5 h; Irradiation; 2: With potassium iodide in ethanol T=20°C; Reduction; 1 h; Title compound not separated from byproducts;
参考文献
El Hafidi; Michel; Bascoul; Crastes De Paulet
Chemistry and Physics of Lipids, 1999 , vol. 100, # 1-2 p. 127 - 138