2-(2-氯苯磺酰基)苯并噻唑合成路线 (共 3 条)
反应条件
iron(III) chloride; sodium t-butanolate; N-methyl-2-(methylamino)ethylamine in toluene
T=135°C; 24 h;
参考文献
Correa, Arkaitz; Carril, Monica; Bolm, Carsten
Angewandte Chemie - International Edition, 2008 , vol. 47, # 15 p. 2880 - 2883
反应条件
copper(l) iodide; 1,10-phenanthroline; oxygen; sulfur; potassium hydroxide in water; dimethyl sulfoxide
T=130°C; 7 h;
参考文献
Wang, Xiaowei; Li, Yanjun; Yuan, Yu
Synthesis (Germany), 2013 , vol. 45, # 9 p. 1247 - 1255
反应条件
CuO; potassium carbonate in N,N-dimethyl-formamide
T=140°C; 48 h; Inert atmosphereSchlenk technique;
参考文献
Rosario, Alisson R.; Casola, Kamila K.; Oliveira, Carla E.S.; Zeni, Gilson
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 14-15 p. 2960 - 2966