1-溴-2-(2-丙烯-1-基氧基)-苯合成路线 （共 50 条）
反应条件
1: 1-allyloxy-2-bromobenzene With tert.-butyl lithium in diethyl ether; pentane
T=-78°C; 0.25 h;
2: With N,N,N',N,-tetramethylethylenediamine in diethyl ether; pentane
T=-78 - -20°C;
3: diphenyldisulfane in diethyl ether; pentane
T=-78 - 20°C; 5.5 h;
参考文献
Barluenga, Jose; Fananas, Francisco J.; Sanz, Roberto; Marcos, Cesar
Chemistry - A European Journal, 2005 , vol. 11, # 18 p. 5397 - 5407
反应条件
triethylsilane; (HS-CH2CH2)-polystyrene
T=70°C; 6 h;
参考文献
Deleuze, Herve; Maillard, Bernard; Mondain-Monval, Olivier
Bioorganic and medicinal chemistry letters, 2002 , vol. 12, # 14 p. 1877 - 1880
反应条件
1: With tert.-butyl lithium in diethyl ether; pentane
T=-78°C; 0.5 h;
2: With N,N,N',N,-tetramethylethylenediamine in diethyl ether; pentane
T=-78°C; 0.5 h; Further stages.;
参考文献
Barluenga, Jose; Fananas, Francisco J.; Sanz, Roberto; Marcos, Cesar
Organic Letters, 2002 , vol. 4, # 13 p. 2225 - 2228
反应条件
sodium tetrahydroborate; di-tert-butyl peroxide in N,N-dimethyl-formamide
T=80°C; 5 h; Irradiation;
参考文献
Abeywickrema, Anil N.; Beckwith, Athelstan L.J.
Tetrahedron Letters, 1986 , vol. 27, # 1 p. 109 - 112
反应条件
[2,2']bipyridinyl; tetra-n-butylammonium tetrafluoroborate; palladium dichloride in N,N-dimethyl-formamide
T=20°C; Reduction; Electrochemical reaction;
参考文献
Franco; Panyella; Rocamora; Gomez; Clinet; Muller; Dunach
Tetrahedron Letters, 1999 , vol. 40, # 31 p. 5685 - 5688
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene
Heating;
参考文献
Togo, Hideo; Kikuchi, Osamu
Heterocycles, 1989 , vol. 28, # 1 p. 373 - 381
反应条件
ammonia; isopropyl alcohol; acetone; potassium tert-butylate in diethyl ether
2 h; Irradiation;
参考文献
Vaillard, Santiago E.; Postigo, Al; Rossi, Roberto A.
Journal of Organic Chemistry, 2004 , vol. 69, # 6 p. 2037 - 2041
反应条件
tetra-n-butylammonium tetrafluoroborate; Ni(cyclam)Br2 in N,N-dimethyl-formamide
T=20°C; Carboxylation; cyclization; P=760 Torr; ElectrolysisMg/Ni electrodes; Product distribution; Further Variations:CatalystsPressuresReaction partnersnature of the electrodes;
参考文献
Olivero; Dunach
European Journal of Organic Chemistry, 1999 , # 8 p. 1885 - 1891
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene
0.5 h; Heating;
参考文献
Togo, Hideo; Kikuchi, Osamu
Tetrahedron Letters, 1988 , vol. 29, # 33 p. 4133 - 4134
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene
Heating;
参考文献
Togo, Hideo; Kikuchi, Osamu
Heterocycles, 1989 , vol. 28, # 1 p. 373 - 381
