2,6-二甲氧基苯基三氟甲磺酸酯合成路线 (共 13 条)
反应条件
pyridine in dichloromethane T=0°C; 0.25 h;
参考文献
Thompson, Alicia L. S.; Kabalka, George W.; Akula, Murthy R.; Huffman, John W.
Synthesis, 2005 , # 4 art. no. M05304SS, p. 547 - 550
反应条件
2,6-di-tert-butyl-4-methyl-phenol; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; lithium chloride in N,N-dimethyl-formamide T=120°C; 7 h;
参考文献
Saa, Jose M.; Martorell, Gabriel; Garcia-Raso, Angel
Journal of Organic Chemistry, 1992 , vol. 57, # 2 p. 678 - 685
反应条件
bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; lithium chloride
参考文献
Martorell, Gabriel; Garcia-Raso, Angel; Saa, Jose M.
Tetrahedron Letters, 1990 , vol. 31, # 16 p. 2357 - 2360
反应条件
tetraethylammonium hydroxide in 1,4-dioxane T=60°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 45, # 33 p. 6317 - 6320
反应条件
pyridine; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate T=150°C; 0.333333 h; microwave irradiation;
参考文献
Synthesis, , # 4 p. 594 - 596
反应条件
bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; lithium chloride
参考文献
Saa, Jose M.; Martorell, Gabriel; Garcia-Raso, Angel
Journal of Organic Chemistry, 1992 , vol. 57, # 2 p. 678 - 685
反应条件
hydrogen; triethylamine; palladium on activated charcoal in methanol P=3361.5 Torr; other solvent, other temp., other reagents, other catalysts;
参考文献
Journal of Organic Chemistry, , vol. 55, # 3 p. 991 - 995
反应条件
1: 93 percent / Et3N / PdCl2(dppf) / dioxane / Heating 2: 77 percent / aq. CuBr2 / methanol / Heating View Scheme
参考文献
Thompson, Alicia L. S.; Kabalka, George W.; Akula, Murthy R.; Huffman, John W.
Synthesis, 2005 , # 4 art. no. M05304SS, p. 547 - 550
反应条件
2,6-di-tert-butyl-4-methyl-phenol; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; lithium chloride in N,N-dimethyl-formamide
T=120°C; 5.5 h;
参考文献
Saa, Jose M.; Martorell, Gabriel; Garcia-Raso, Angel
Journal of Organic Chemistry, 1992 , vol. 57, # 2 p. 678 - 685
反应条件
bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; lithium chloride
参考文献
Martorell, Gabriel; Garcia-Raso, Angel; Saa, Jose M.
Tetrahedron Letters, 1990 , vol. 31, # 16 p. 2357 - 2360