1: 3,3-dimethylbutyric acid ethyl ester With lithium diisopropyl amide in tetrahydrofuran; cyclohexane; ethylbenzene T=-78°C; 1.16667 h; Cooling with acetone-dry ice; 2: methyl iodide in tetrahydrofuran; cyclohexane; ethylbenzene T=-78 - 20°C; 17.5 h; Cooling with acetone-dry ice;

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lithium aluminium tetrahydride in tetrahydrofuran; diethyl ether; ethylbenzene T=0°C; 16 h;