2'-羟基-2,4,4,7,4'-五甲基黄烷合成路线 （共 3 条）
反应条件
hydrogen; nickel T=180 - 280°C;
参考文献
Schering-Kahlbaum A.G.
Patent: US1838454 , 1929 ;
Full Text Show Details
Schering-Kahlbaum A.G.
Patent: DE556162 , 1929 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 2961
Full Text Show Details
Schering-Kahlbaum A.G.
Patent: DE554646 , 1926 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 2526
反应条件
sodium hydroxide in ethylene glycol
Ring cleavage; condensation; 2.5 h; Heatingacid hydrolysis;
参考文献
Kamat, Vijayendra P.; Asolkar, Ratnakar N.; Kirtany, Janardan K.
Synthetic Communications, 1998 , vol. 28, # 24 p. 4581 - 4587
反应条件
methanesulfonic acid
T=19.85 - 139.85°C; Condensation; 129 h;
参考文献
Ejsmont, Krzysztof; Kyziol, Janusz; Nowakowska, Ewa; Zaleski, Jacek
Acta Crystallographica Section C: Crystal Structure Communications, 2000 , vol. 56, # 1 p. 93 - 94
