2,3,4,5,6-五氟苯甲酸合成路线 （共 133 条）
反应条件
sodium tetrahydroborate; zinc(II) chloride in diethylene glycol dimethyl ether 5 h; Reflux;
参考文献
Zhang, Deyan; Chen, Zizhan; Cai, Huihua; Zou, Xinzhuo
Journal of Fluorine Chemistry, 2009 , vol. 130, # 10 p. 938 - 941
反应条件
1.1: Mg / bis-(2-methoxy-ethyl) ether / 4 h / 60 - 80 °C 1.2: bis-(2-methoxy-ethyl) ether / 2 h / 100 °C 2.1: HBr / 12 h / Heating View Scheme
参考文献
Bazyl'; Kisil'; Burgart; Saloutin; Chupakhin
Journal of Fluorine Chemistry, 1999 , vol. 94, # 1 p. 11 - 13
反应条件
sulfuric acid in tetrachloromethane Heating;
参考文献
Keana, John F. W.; Cai, Sui Xiong
Journal of Organic Chemistry, 1990 , vol. 55, # 11 p. 3640 - 3647
反应条件
hydrogen fluoride; SbF5 T=95°C; 15 h; Title compound not separated from byproducts.;
参考文献
Zonov, Yaroslav V.; Karpov, Victor M.; Platonov, Vyacheslav E.; Rybalova, Tatjana V.; Gatilov, Yuri V.
Journal of Fluorine Chemistry, 2006 , vol. 127, # 12 p. 1574 - 1583
反应条件
triphenylphosphine; silver carbonate; palladium dichloride in dimethyl sulfoxide T=130°C; 6 h; Inert atmosphere;
参考文献
Xie, Kai; Wang, Sizhuo; Yang, Zhiyong; Liu, Jidan; Wang, Anwei; Li, Xiujian; Tan, Ze; Guo, Can-Cheng; Deng, Wei
European Journal of Organic Chemistry, 2011 , # 29 p. 5787 - 5790
反应条件
triphenylphosphine; silver carbonate; palladium dichloride in dimethyl sulfoxide T=130°C; 6 h; Inert atmosphere;
参考文献
Xie, Kai; Wang, Sizhuo; Yang, Zhiyong; Liu, Jidan; Wang, Anwei; Li, Xiujian; Tan, Ze; Guo, Can-Cheng; Deng, Wei
European Journal of Organic Chemistry, 2011 , # 29 p. 5787 - 5790
反应条件
triphenylphosphine; silver carbonate; palladium dichloride in dimethyl sulfoxide T=130°C; 6 h; Inert atmosphere;
参考文献
Xie, Kai; Wang, Sizhuo; Yang, Zhiyong; Liu, Jidan; Wang, Anwei; Li, Xiujian; Tan, Ze; Guo, Can-Cheng; Deng, Wei
European Journal of Organic Chemistry, 2011 , # 29 p. 5787 - 5790
反应条件
[Fe(II)(TPA)(CH3CN)2](OTf)2; water; dihydrogen peroxide in acetonitrile T=20°C;
参考文献
Das, Parthapratim; Que Jr., Lawrence
Inorganic Chemistry, 2010 , vol. 49, # 20 p. 9479 - 9485
反应条件
[Fe(II)(TPA)(CH3CN)2](OTf)2; water; dihydrogen peroxide in acetonitrile T=20°C;
参考文献
Das, Parthapratim; Que Jr., Lawrence
Inorganic Chemistry, 2010 , vol. 49, # 20 p. 9479 - 9485
反应条件
[Fe(II)(TPA)(CH3CN)2](OTf)2; water; dihydrogen peroxide in acetonitrile T=20°C;
参考文献
Das, Parthapratim; Que Jr., Lawrence
Inorganic Chemistry, 2010 , vol. 49, # 20 p. 9479 - 9485
