1,1'-联-2-萘酚合成路线 (共 233 条)
反应条件
hydrogenchloride in ethanol; water T=50°C; 3 h;
参考文献
Masters, Kye-Simeon; Braese, Stefan
Angewandte Chemie - International Edition, 2013 , vol. 52, # 3 p. 866 - 869
Angew. Chem., 2013 , vol. 125, # 3 p. 899 - 903,5
反应条件
copper (II) acetate monohydrate in para-xylene T=130°C; 1 h; Green chemistry;
参考文献
Deb, Mohit L.; Dey, Suvendu S.; Bento, Isabel; Barros, M. Teresa; Maycock, Christopher D.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 37 p. 9791 - 9795
Angew. Chem., 2013 , vol. 125, # 37 p. 9973 - 9977,5
反应条件
copper dichloride T=50 - 55°C; 0.583333 h; Neat (no solvent);
参考文献
Asian Journal of Chemistry, , vol. 23, # 7 p. 3097 - 3100
反应条件
tert-butylamine; copper dichloride in methanol T=50°C; oxidative cross-coupling; 0.75 h;
参考文献
Hovorka, Martin; Zavada, Jiri
Organic Preparations and Procedures International, 1991 , vol. 23, # 2 p. 200 - 203
反应条件
tert-butylamine; copper dichloride in isopropyl alcohol T=50°C; 2 h; Yields of byproduct given;
参考文献
Hovorka; Scigel; Gunterova; Tichy; Zavada
Tetrahedron, 1992 , vol. 48, # 43 p. 9503 - 9516
反应条件
oxygen; (-)-2,2′-isopropylidenebis[(4S)-4-phenyl-2-oxazoline]; copper(l) chloride in tetrahydrofuran T=20°C; 3 h;
参考文献
Temma, Tomohisa; Habaue, Shigeki
Tetrahedron Letters, 2005 , vol. 46, # 34 p. 5655 - 5657
反应条件
NbCl5 in toluene 0.5 h; Heating;
参考文献
European Journal of Organic Chemistry, , # 3 p. 752 - 758
反应条件
1: (S)-6,6'-dibromo-2,2'-dihydroxy-1,1'-binaphthyl With n-butyllithium in tetrahydrofuran; hexane T=-78 - -70°C; 5 h; Inert atmosphere; 2: 1,2-epoxy-2-methyl-propane With boron trifluoride diethyl etherate in tetrahydrofuran; hexane T=-78 - -40°C; 2 h; Inert atmosphere; 3: With hydrogenchloride in tetrahydrofuran; hexane; water T=20°C; pH=< 1; Cooling with ice;
参考文献
Journal of Organic Chemistry, , vol. 76, # 7 p. 2319 - 2323
反应条件
anhydrous iron chloride; 1,10-phenanthroline; di-tert-butyl peroxide in 1,2-dichloro-ethane T=70°C; 1 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 14, # 13 p. 3324 - 3327
反应条件
boron trichloride in dichloromethane 1 h; 0 deg C - room temperature;
参考文献
Journal of Organic Chemistry, , vol. 61, # 8 p. 2695 - 2698