叔-丁基 (3-methoxyphenyl)氨基甲酸酯合成路线 （共 11 条）
反应条件
Cu(BF4)2 T=30 - 33°C; 0.166667 h;
参考文献
Lochner, Martin; Mu, Linjing; Woggon, Wolf-D.
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 6-7 p. 743 - 765
反应条件
palladium diacetate; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in 1,4-dioxane T=100°C; 4 h; Inert atmosphere;
参考文献
Qin, Lijin; Cui, Hongmeng; Zou, Dapeng; Li, Jingya; Wu, Yangjie; Zhu, Zhiwu; Wu, Yusheng
Tetrahedron Letters, 2010 , vol. 51, # 33 p. 4445 - 4448
反应条件
BiBr3; water in acetonitrile T=20°C; 1 h;
参考文献
Zheng, Jianlong; Yin, Biaolin; Huang, Wenming; Li, Xiaopeng; Yao, Hequan; Liu, Zhaogui; Zhang, Jiancun; Jiang, Sheng
Tetrahedron Letters, 2009 , vol. 50, # 36 p. 5094 - 5097
反应条件
methanol; tris(acetonitrile)(tricarbonyl)molybdenum T=130°C; 0.25 h; Microwave irradiationInert atmosphere; chemoselective reaction;
参考文献
Nielsen, Simon Dalsgaard; Smith, Garrick; Begtrup, Mikael; Kristensen, Jesper L.
European Journal of Organic Chemistry, 2010 , # 19 p. 3704 - 3710
反应条件
2-(di-tert-butylphosphino)-2'-isopropoxy-1,1'-binaphthyl; caesium carbonate; bis(dibenzylideneacetone)-palladium(0) in tert-butyl alcohol T=100°C; 20 h; Inert atmosphere;
参考文献
Ma, Fangfang; Xie, Xiaomin; Zhang, Lei; Peng, Zhiyong; Ding, Lina; Fu, Lei; Zhang, Zhaoguo
Journal of Organic Chemistry, 2012 , vol. 77, # 12 p. 5279 - 5285
反应条件
1: 1) t-BuLi / 1) THF, 2) r.t., 6 h 2: conc. HCl / tetrahydrofuran View Scheme
参考文献
Gould; Eisenberg
Journal of Organic Chemistry, 1991 , vol. 56, # 23 p. 6666 - 6671
反应条件
2: 95 percent / 6 N HCl / acetic acid / 2 h / Ambient temperature 3: LiSMe / dimethylformamide / 6 h / 80 °C View Scheme
参考文献
Gould; Eisenberg
Journal of Organic Chemistry, 1991 , vol. 56, # 23 p. 6666 - 6671
反应条件
1: 1) t-BuLi / 1) THF, 2) r.t., 6 h
2: conc. HCl / tetrahydrofuran
View Scheme
参考文献
Gould; Eisenberg
Journal of Organic Chemistry, 1991 , vol. 56, # 23 p. 6666 - 6671
反应条件
1.1: tert.-butyl lithium / diethyl ether / -78 - -20 °C
1.2: -78 - -65 °C
2.1: trifluoroacetic acid / dichloromethane / 0 - 20 °C / Darkness
View Scheme
参考文献
Wu, Wenbin; Li, Zheng; Zhou, Guangbiao; Jiang, Sheng
Tetrahedron Letters, 2011 , vol. 52, # 19 p. 2488 - 2491
反应条件
1: 1) t-BuLi / 1) THF, 2) r.t., 6 h
2: conc. HCl / tetrahydrofuran
3: LiSMe / dimethylformamide / 24 h / 95 °C
View Scheme
参考文献
Gould; Eisenberg
Journal of Organic Chemistry, 1991 , vol. 56, # 23 p. 6666 - 6671
