反应条件
in diethyl ether; benzene byproducts: (CH3COCHCOCH3)MgCl; Grignard reagent:Gmelin educt in 2:1 molar ratio, reflux for 2-3 h; by-product filtered off, solvent distd. off, product vac. distd.;
参考文献
Chandrasekaran, R. K.; Venkataraman, S.; Koola, Johnson D.
Journal of Organometallic Chemistry, 1981 , vol. 215, # 3 p. C43 - C44