苯丙酮乙烷-1,2-二基二硫代缩醛合成路线 （共 6 条）
反应条件
silica gel; copper(II) nitrate in tetrachloromethane 0.25 h; Ambient temperature;
参考文献
Lee, Jong Gun; Hwang, Je Pil
Chemistry Letters, 1995 , # 7 p. 507 - 508
反应条件
lithium diisopropyl amide 1.) THF, -15 deg C, 1 h, 2.) THF, a) -10 to -5 deg C, b) RT, 24 h; Yield given. Multistep reaction;
参考文献
Ikehira, Hideyuki; Tanimoto, Shigeo; Oida, Tatsuo
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 8 p. 2537 - 2538
反应条件
tert-butylhypochlorite in tetrachloromethane T=20°C; 0.116667 h;
参考文献
Arote, Nitin D.; Telvekar, Vikas N.; Akamanchi
Synlett, 2005 , # 19 art. no. D25105ST, p. 2935 - 2938
反应条件
sodium tetrahydroborate; NiII chloride hexahydrate in tetrahydrofuran; methanol T=20°C; 0.416667 h;
参考文献
Khurana, Jitender M.; Magoo, Devanshi
Synthetic Communications, 2010 , vol. 40, # 19 p. 2908 - 2913
反应条件
N-iodo-succinimide; hexafluoropropylene; diethylamine in dichloromethane; water
T=-78 - -20°C; 1 h;
参考文献
Shimizu, Makoto; Maeda, Takashi; Fujisawa, Tamotsu
Journal of Fluorine Chemistry, 1995 , vol. 71, # 1 p. 9 - 12
反应条件
lithium diisopropyl amide
1.) THF, -15 deg C, 1 h, 2.) THF, a) -10 to -5 deg C, b) RT, 24 h; Yield given. Multistep reaction;
参考文献
Ikehira, Hideyuki; Tanimoto, Shigeo; Oida, Tatsuo
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 8 p. 2537 - 2538
