反应条件
lithium aluminium tetrahydride; n-butyllithium
1.) THF/hexane, -78 deg C, 30 min, 2.) THF/hexane, -78 -> -10 deg C, 3.) THF, RT, 6 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Hammer, Kristin; Benneche, Tore; Hope, Hakon; Undheim, Kjell
Acta Chemica Scandinavica, 1997 , vol. 51, # 3 SUPPL. p. 392 - 402
