alpha-氧代噻吩-2-乙腈合成路线 （共 8 条）
参考文献
Steinkopf; Thormann
Justus Liebigs Annalen der Chemie, 1939 , vol. 540, p. 1,5
反应条件
zinc(II) iodide; PEG400 in dichloromethane
T=20°C; 5 h;
参考文献
Cao, Yu-Qing; Du, Yun-Fei; Chen, Bao-Hua; Li, Ji-Tai
Synthetic Communications, 2004 , vol. 34, # 16 p. 2951 - 2957
反应条件
PEG-400; potassium iodide; silver(I) in N,N-dimethyl-formamide
T=20°C; 9 h;
参考文献
Li, Zheng; Shi, Shengyi; Yang, Jingya
Synlett, 2006 , # 15 p. 2495 - 2497
反应条件
tert.-butylhydroperoxide; tris(triphenylphosphine)ruthenium(II) chloride in water; benzene
T=22°C; 1 h;
参考文献
Tanaka, Masato; Kobayashi, Toshi-aki; Sakakura, Toshiyasu
Angewandte Chemie, 1984 , vol. 96, # 7 p. 519 - 520
反应条件
in neat (no solvent)
T=75°C; 0.0833333 h;
参考文献
Tanaka, Masato
Tetrahedron Letters, 1980 , vol. 21, p. 2959 - 2962
反应条件
(Ph3P)2Pd(Ph)(I) in tetrahydrofuran
T=100°C; P=6080 Torr; 24 h;
参考文献
Tanaka, Masato
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 2 p. 637 - 638
反应条件
acetyl chloride
anschliessend Erhitzen unter vermindertem Druck;
参考文献
Steinkopf; Thormann
Justus Liebigs Annalen der Chemie, 1939 , vol. 540, p. 1,5
反应条件
1: aq.-ethanolic NaOH-solution
2: aqueous sulfuric acid
View Scheme
参考文献
Cagniant; Cagniant
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1949 , vol. 229, p. 1150
