2-溴-1,3-环己二酮合成路线 （共 16 条）
反应条件
disodium hydrogenphosphate; [Ir(phenylpyridine(-1H))2(4,4′-di-tert-butyl-2,2′-bipyridine)](PF6) in ethanol T=20°C; 12 h; Inert atmosphereIrradiation; Catalytic behavior; Reagent/catalystSolvent;
参考文献
Jiang, Heng; Cheng, Yuanzheng; Zhang, Yan; Yu, Shouyun
Organic Letters, 2013 , vol. 15, # 18 p. 4884 - 4887
反应条件
pyridine T=50°C; Hantzsch Synthesis;
参考文献
Bayer CropScience AG
Patent: US2009/30024 A1, 2009 ;
Location in patent: Page/Page column 36-37 ;
反应条件
pyridine in methanol 3.5 h; Reflux;
参考文献
McIntyre, Neil A.; McInnes, Campbell; Griffiths, Gary; Barnett, Anna L.; Kontopidis, George; Slawin, Alexandra M. Z.; Jackson, Wayne; Thomas, Mark; Zheleva, Daniella I.; Wang, Shudong; Blake, David G.; Westwood, Nicholas J.; Fischer, Peter M.
Journal of Medicinal Chemistry, 2010 , vol. 53, # 5 p. 2136 - 2145
反应条件
thiourea in tetrahydrofuran; 1,4-dioxane; water
参考文献
BASF Aktiengesellschaft Ludwigshafen, Germany
Patent: US2003/153568 A1, 2003 ;
反应条件
1-methyl-1H-imidazole in water; isopropyl alcohol T=20°C; 2 h;
参考文献
Meshram; Thakur, Pramod B.; Madhu Babu; Bangade, Vikas M.
Tetrahedron Letters, 2012 , vol. 53, # 39 p. 5265 - 5269
反应条件
1: ethyl magnesium bromide; diethyl ether
2: aqueous NaOH
View Scheme
参考文献
Nasarow; Saw'jalow
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1958 , p. 200,202; engl. Ausg. S. 186, 187
