N-苯基-3-氯苯甲酰胺合成路线 （共 29 条）
反应条件
air; copper(II) bis(trifluoromethanesulfonate) in 1,2-dichloro-benzene T=160°C; P=760.051 Torr; 28 h; regioselective reaction;
参考文献
Ueda, Satoshi; Nagasawa, Hideko
Journal of Organic Chemistry, 2009 , vol. 74, # 11 p. 4272 - 4277
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=-10°C; 0.138889 h; Inert atmosphere; 2: With acetic acid in tetrahydrofuran; hexane T=-5°C; 0.0166667 h; Ionic liquid;
参考文献
Sedelmeier, Joerg; Lima, Fabio; Litzler, Alain; Martin, Benjamin; Venturoni, Francesco
Organic Letters, 2013 , vol. 15, # 21 p. 5546 - 5549
反应条件
sulfuryl dichloride; benzene
参考文献
Jadhav; Sukhtankar
Journal of the Indian Chemical Society, 1938 , vol. 15, p. 649,651
反应条件
magnesium oxide in neat (no solvent)
T=70°C; 0.25 h; Green chemistry; chemoselective reaction;
参考文献
Das, Vijay Kumar; Devi, Rashmi Rekha; Thakur, Ashim Jyoti
Applied Catalysis A: General, 2013 , vol. 456, p. 118 - 125
反应条件
potassium phosphate; N-methyl-2-(methylamino)ethylamine; iron(III) chloride in toluene
T=135°C; 24 h;
参考文献
Correa, Arkaitz; Bolm, Carsten
Angewandte Chemie - International Edition, 2007 , vol. 46, # 46 p. 8862 - 8865
反应条件
oxygen; sodium hydroxide in tetrahydrofuran; water
T=25°C; 12 h;
参考文献
Soule, Jean-Francois; Miyamura, Hiroyuki; Kobayashi, Shu
Chemistry - An Asian Journal, 2013 , vol. 8, # 11 p. 2614 - 2626
反应条件
di-tert-butyl peroxide; potassium hydroxide in chlorobenzene
T=140°C; 24 h;
参考文献
Xiao, Fuhong; Liu, Yong; Tang, Chenglin; Deng, Guo-Jun
Organic Letters, 2012 , vol. 14, # 4 p. 984 - 987
反应条件
triethylamine in ethyl acetate
T=0 - 20°C; 4 h;
参考文献
Ueda, Satoshi; Nagasawa, Hideko
Journal of Organic Chemistry, 2009 , vol. 74, # 11 p. 4272 - 4277
反应条件
copper(l) iodide; manganese(II) fluoride; rel-(R,R)-DACH; potassium hydroxide in water
T=100°C; 24 h;
参考文献
Teo, Yong-Chua; Yong, Fui-Fong; Ithnin, Idzham Khalid; Yio, Siew-Hui Trionna; Lin, Zhiyin
European Journal of Organic Chemistry, 2013 , # 3 p. 515 - 524
反应条件
triethylamine; acrylic acid methyl ester; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide
T=80°C; 24 h; Yield given. Title compound not separated from byproducts;
参考文献
Mahanty, Jyan S.; De, Mahuya; Kundu, Nitya G.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 17 p. 2577 - 2579
