Z-13-十八烯-1-乙酸酯合成路线 (共 8 条)
反应条件
pyridine
24 h; Ambient temperature;
参考文献
Subbaraman, A S; Mithran, S; Mamdapur, V R
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 9 p. 865 - 866
反应条件
1: 91 percent / 30percent H2O2, HCOOH
2: 89 percent / aq. Na2CO3, H3PO4, NaIO4
3: 1.) NaH, DMSO
4: PTS
5: 90 percent / LiAlH4 (LAH) / diethyl ether
6: 100 percent / pyridine / 24 h / Ambient temperature
View Scheme
参考文献
Subbaraman, A S; Mithran, S; Mamdapur, V R
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 9 p. 865 - 866
反应条件
1: 89 percent / aq. Na2CO3, H3PO4, NaIO4
2: 1.) NaH, DMSO
3: PTS
4: 90 percent / LiAlH4 (LAH) / diethyl ether
5: 100 percent / pyridine / 24 h / Ambient temperature
View Scheme
参考文献
Subbaraman, A S; Mithran, S; Mamdapur, V R
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 9 p. 865 - 866
反应条件
1: 1.) NaH, DMSO
2: PTS
3: 90 percent / LiAlH4 (LAH) / diethyl ether
4: 100 percent / pyridine / 24 h / Ambient temperature
View Scheme
参考文献
Subbaraman, A S; Mithran, S; Mamdapur, V R
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 9 p. 865 - 866
反应条件
1: PTS
2: 90 percent / LiAlH4 (LAH) / diethyl ether
3: 100 percent / pyridine / 24 h / Ambient temperature
View Scheme
参考文献
Subbaraman, A S; Mithran, S; Mamdapur, V R
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 9 p. 865 - 866
反应条件
1: 90 percent / LiAlH4 (LAH) / diethyl ether
2: 100 percent / pyridine / 24 h / Ambient temperature
View Scheme
参考文献
Subbaraman, A S; Mithran, S; Mamdapur, V R
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 9 p. 865 - 866
反应条件
1: 54 percent / Li2CuCl4 / tetrahydrofuran / 3 h / -10 °C
2: 53 percent / pyridinium p-toluenesulfonate / methanol / 6 h / 55 °C
3: 86 percent / pyridine / CH2Cl2 / 5 h / Ambient temperature
View Scheme
参考文献
Trehan; Vig; Singh; Sharma; Kad
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 6 p. 518 - 520
反应条件
1: 53 percent / pyridinium p-toluenesulfonate / methanol / 6 h / 55 °C
2: 86 percent / pyridine / CH2Cl2 / 5 h / Ambient temperature
View Scheme
参考文献
Trehan; Vig; Singh; Sharma; Kad
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 6 p. 518 - 520