[[(2-羟基乙基)亚氨基]二(亚甲基)]二膦酸合成路线 (共 19 条)
参考文献
Makaranets, B.I.; Polynova, T.N.; Porai-Koshits, M.A.; Il'ichev, S.A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 11 p. 2430
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 11 p. 2649
反应条件
1: in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=185°C; 17 h;
2: With hydrogenchloride in water
T=90°C; 16 h;
参考文献
Monsanto Technology LLC
Patent: US2005/54871 A1, 2005 ;
Location in patent: Page/Page column 31 ;
反应条件
sodium hydroxide in water
T=100°C; 6 h;
参考文献
Tsirul'nikova, N. V.; Temkina, V. Ya.; Sushitskaya, T. M.; Rykov, S. V.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 5 p. 1028 - 1035,859 - 864
反应条件
T=153°C; 24 h; Molecular sieve;
参考文献
Monsanto Technology LLC
Patent: US2005/54871 A1, 2005 ;
Location in patent: Page/Page column 32 ;
反应条件
sodium hydroxide; water in ethanol
T=10 - 75°C; 3 h; Product distribution / selectivity;
参考文献
Thermphos Trading GmbH
Patent: EP1932848 A1, 2008 ;
Location in patent: Page/Page column 6 ;
反应条件
sodium hydroxide; water
T=10 - 100°C; 3.66667 h; Product distribution / selectivity;
参考文献
Thermphos Trading GmbH
Patent: EP1932848 A1, 2008 ;
Location in patent: Page/Page column 4 ;
反应条件
sodium sulfide; sodium hydroxide; water
T=10 - 80°C; 4 h; Product distribution / selectivity;
参考文献
Thermphos Trading GmbH
Patent: EP1932848 A1, 2008 ;
Location in patent: Page/Page column 6 ;
反应条件
sodium hydroxide; ammonia; water
T=6 - 95°C; 5 h; Product distribution / selectivity;
参考文献
Thermphos Trading GmbH
Patent: EP1932848 A1, 2008 ;
Location in patent: Page/Page column 5; 7 ;
反应条件
sodium hydroxide; ammonia; water
T=6 - 95°C; 6.5 h; Product distribution / selectivity;
参考文献
Thermphos Trading GmbH
Patent: EP1932848 A1, 2008 ;
Location in patent: Page/Page column 5 ;
反应条件
sodium hydroxide; ammonia; water
T=6 - 95°C; 4 h; Product distribution / selectivity;
参考文献
Thermphos Trading GmbH
Patent: EP1932848 A1, 2008 ;
Location in patent: Page/Page column 5 ;