N-对甲苯基-对甲苯磺胺合成路线 （共 64 条）
反应条件
1: bis(4-methylphenyl)-disulfide With dihydrogen peroxide; zirconium tetrachloride in acetonitrile
T=25°C;
2: p-toluidine With pyridine in acetonitrile
T=25°C; 0.0333333 h; chemoselective reaction;
参考文献
Bahrami, Kiumars; Khodaei, Mohammad M.; Soheilizad, Mehdi
Tetrahedron Letters, 2010 , vol. 51, # 37 p. 4843 - 4846
反应条件
1: para-thiocresol With dihydrogen peroxide; zirconium tetrachloride in acetonitrile
T=25°C;
2: p-toluidine With pyridine in acetonitrile
T=25°C; 0.0333333 h; chemoselective reaction;
参考文献
Bahrami, Kiumars; Khodaei, Mohammad M.; Soheilizad, Mehdi
Tetrahedron Letters, 2010 , vol. 51, # 37 p. 4843 - 4846
反应条件
copper(l) iodide; N-methyl-2-(methylamino)ethylamine in 1,4-dioxane
T=100 - 110°C; 8 h; Inert atmosphere;
参考文献
Hosseinzadeh, Rahman; Tajbakhsh, Mahmood; Mohadjerani, Maryam; Alikarami, Mohammad
Journal of Chemical Sciences, 2010 , vol. 122, # 2 p. 143 - 148
反应条件
potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); di-tert-butyl(2′,4′,6′-triisopropylbiphenyl-2-yl)phosphine in 1,1-dimethylpropan-1-ol
T=80°C; 16 h; Inert atmosphere;
参考文献
Shekhar, Shashank; Dunn, Travis B.; Kotecki, Brian J.; Montavon, Donna K.; Cullen, Steven C.
Journal of Organic Chemistry, 2011 , vol. 76, # 11 p. 4552 - 4563
反应条件
potassium phosphate; copper(l) iodide; N,N-dimethylaminoacetic acid in N,N-dimethyl-formamide
48 h; Heating;
参考文献
Deng, Wei; Liu, Lei; Zhang, Chen; Liu, Min; Guo, Qing-Xiang
Tetrahedron Letters, 2005 , vol. 46, # 43 p. 7295 - 7298
反应条件
copper(l) iodide; 1,10-phenanthroline; Cu; potassium carbonate in N,N-dimethyl-formamide
T=110°C; 24 h;
参考文献
Yavari; Solgi; Ghazanfarpour-Darjani; Ahmadian
Journal of the Iranian Chemical Society, 2012 , vol. 9, # 6 p. 977 - 981
反应条件
hydrogenchloride; water; sodium acetate; sodium hydrogencarbonate; acetic acid in ethanol
T=60°C; 24 h; Yield given;
参考文献
Ono, Machiko; Tamura, Shinzo
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1453 - 1462
反应条件
hydrogenchloride; water; sodium acetate; sodium hydrogencarbonate; acetic acid in 1,4-dioxane; water
T=100°C; 3.5 h;
参考文献
Ono, Machiko; Tamura, Shinzo
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1453 - 1462
反应条件
FeCl3·6H2O
T=60°C; 4 h; Inert atmosphere;
参考文献
Bunce, Richard A.; Cain, Nicholas R.; Cooper, John G.
Organic Preparations and Procedures International, 2013 , vol. 45, # 1 p. 28 - 43
反应条件
methanol; sodium hydroxide; sodium hydrogencarbonate in tetrahydrofuran
T=60°C; 2.1 h;
参考文献
Ono, Machiko; Tamura, Shinzo
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1453 - 1462
